3-(6,7-methylenedioxy-4-oxo-1,4-dihydroquinolin-2-yl)-5-methoxyphenyl dihydrogen phosphate

Base Information

Chemical Name:3-(6,7-methylenedioxy-4-oxo-1,4-dihydroquinolin-2-yl)-5-methoxyphenyl dihydrogen phosphate
CAS No.:1355235-84-5
Molecular Formula:C₁₇H₁₄NO₈P
Molecular Weight:391.274
Hs Code.:

Synonyms:3-(6,7-methylenedioxy-4-oxo-1,4-dihydroquinolin-2-yl)-5-methoxyphenyl dihydrogen phosphate

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Chemical Property of 3-(6,7-methylenedioxy-4-oxo-1,4-dihydroquinolin-2-yl)-5-methoxyphenyl dihydrogen phosphate

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Technology Process of 3-(6,7-methylenedioxy-4-oxo-1,4-dihydroquinolin-2-yl)-5-methoxyphenyl dihydrogen phosphate

There total 12 articles about 3-(6,7-methylenedioxy-4-oxo-1,4-dihydroquinolin-2-yl)-5-methoxyphenyl dihydrogen phosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: dibenzyl 3-(6,7-methylenedioxyquinolin-2-yl)-5-methoxyphenyl phosphate

: 1355235-84-5
3-(6,7-methylenedioxy-4-oxo-1,4-dihydroquinolin-2-yl)-5-methoxyphenyl dihydrogen phosphate

Guidance literature:: With palladium 10% on activated carbon; hydrogen; In methanol; at 25 ℃; for 0.25h;
DOI:10.3390/molecules18078028

Reference yield: 80.0%

: 1355235-83-4
2-(3-([bis-[(benzyl)oxy]]phosphoryl)oxy-5-methoxyphenyl)-6,7-methylenedioxyquinolin-4-one

: 1355235-84-5
2-(3-(dihydrogen)phosphate-5-methoxyphenyl)-6,7-methylenedioxy-quinolin-4-one

Guidance literature:: 2-(3-([bis-[(benzyl)oxy]]phosphoryl)oxy-5-methoxyphenyl)-6,7-methylenedioxyquinolin-4-one; With hydrogen; palladium 10% on activated carbon; In methanol; at 20 ℃; for 0.25h;

With sodium hydrogencarbonate; In water;

With hydrogenchloride; In water;

Reference yield:

: 50637-26-8
methyl 3-(benzyloxy)-5-methoxybenzoate

: 1355235-84-5
2-(3-(dihydrogen)phosphate-5-methoxyphenyl)-6,7-methylenedioxy-quinolin-4-one

Guidance literature:: Multi-step reaction with 8 steps

1: sodium hydroxide; water / ethanol / 1 h / Reflux

2: N,N-dimethyl-formamide; thionyl chloride / toluene

3: triethylamine / tetrahydrofuran / 24 h / 20 °C

4: sodium hydroxide / 1,4-dioxane / 24 h / Reflux

5: hydrogen / palladium 10% on activated carbon / methanol / 24 h / 20 °C

6: sodium hydride / tetrahydrofuran; mineral oil / 0.17 h / 20 °C

7: methanol / 48 h / 25 °C

8: hydrogen / palladium 10% on activated carbon / methanol / 0.25 h / 20 °C

With thionyl chloride; water; hydrogen; sodium hydride; triethylamine; N,N-dimethyl-formamide; sodium hydroxide; palladium 10% on activated carbon; In tetrahydrofuran; 1,4-dioxane; methanol; ethanol; toluene; mineral oil;