Diethyl 2-adamantylidenesuccinate

Base Information

Chemical Name:Diethyl 2-adamantylidenesuccinate
CAS No.:70477-64-4
Molecular Formula:C₁₈H₂₆O₄
Molecular Weight:306.402
Hs Code.:
DSSTox Substance ID:DTXSID60466300
Nikkaji Number:J1.522.754K
Mol file:70477-64-4.mol

Synonyms:DIETHYL 2-ADAMANTYLIDENESUCCINATE;70477-64-4;Diethyl 2-(2-adamantylidene)butanedioate;DIETHYL2-ADAMANTYLIDENESUCCINATE;SCHEMBL4379762;DTXSID60466300;diethyl adamant-2-ylidenesuccinate;Diethyl 2-(tricyclo[3.3.1.1~3,7~]decan-2-ylidene)butanedioate

Suppliers and Price of Diethyl 2-adamantylidenesuccinate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
DIETHYL-2-ADAMANTYLIDENESUCCINATE 98.00%
5MG
$ 504.76

Total 5 raw suppliers

Chemical Property of Diethyl 2-adamantylidenesuccinate

Chemical Property:

PSA：52.60000
LogP:3.25540
XLogP3:3.4
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:7
Exact Mass:306.18310931
Heavy Atom Count:22
Complexity:461

Purity/Quality:

99% ^*data from raw suppliers

DIETHYL-2-ADAMANTYLIDENESUCCINATE 98.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCOC(=O)CC(=C1C2CC3CC(C2)CC1C3)C(=O)OCC

Technology Process of Diethyl 2-adamantylidenesuccinate

There total 1 articles about Diethyl 2-adamantylidenesuccinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

: 700-58-3
2-Adamantanone

: 123-25-1
succinic acid diethyl ester

: 70477-64-4
diethyl adamantylidene succinate

Guidance literature:: 2-Adamantanone; succinic acid diethyl ester; With potassium tert-butylate; In tert-butyl alcohol; for 24h; Heating;

With hydrogenchloride; ethanol; Further stages.;
DOI:10.1021/jo005722n

Reference yield:

: 70477-64-4
diethyl adamantylidene succinate

: 94856-25-4
(E)-4-adamantylidene-3-<1-(2,5-dimethyl-3-furyl)ethylidene>tetrahydrofuran-2,5-dione

Guidance literature:: Multi-step reaction with 3 steps

1: lithium diisopropylamide

2: hydrolysis

3: dehydrative cyclization

With lithium diisopropyl amide;