Methyl 1-(2-Methanesulfonyloxyethyl)-3-methoxycarbonyl-4-(2-phenylethyl)pyrrole-2-acetate

Base Information

• Chemical Name: Methyl 1-(2-Methanesulfonyloxyethyl)-3-methoxycarbonyl-4-(2-phenylethyl)pyrrole-2-acetate
• CAS No.: 76209-54-6
• Molecular Formula: C₂₀H₂₅NO₇S
• Molecular Weight: 423.487

Synonyms:Methyl 1-(2-Methanesulfonyloxyethyl)-3-methoxycarbonyl-4-(2-phenylethyl)pyrrole-2-acetate

Chemical Property of Methyl 1-(2-Methanesulfonyloxyethyl)-3-methoxycarbonyl-4-(2-phenylethyl)pyrrole-2-acetate

Chemical Property:

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Technology Process of Methyl 1-(2-Methanesulfonyloxyethyl)-3-methoxycarbonyl-4-(2-phenylethyl)pyrrole-2-acetate

There total 1 articles about Methyl 1-(2-Methanesulfonyloxyethyl)-3-methoxycarbonyl-4-(2-phenylethyl)pyrrole-2-acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

Methyl 1-(2-Hydroxyethyl)-3-methoxycarbonyl-4-(2-phenylethyl)pyrrole-2-acetate (76209-53-5) + methanesulfonyl chloride (124-63-0) → Methyl 1-(2-Methanesulfonyloxyethyl)-3-methoxycarbonyl-4-(2-phenylethyl)pyrrole-2-acetate (76209-54-6)

Guidance literature:

With trimethylamine; In dichloromethane; at 0 ℃; for 0.5h;

DOI:10.1002/jhet.5570170546

Reference yield: 91.0%

Methyl 1-(2-Methanesulfonyloxyethyl)-3-methoxycarbonyl-4-(2-phenylethyl)pyrrole-2-acetate (76209-54-6) → Methyl 1-(2-Chloroethyl)-3-methoxycarbonyl-4-(2-phenylethyl)pyrrole-2-acetate (76209-55-7)

Guidance literature:

With lithium chloride; In N,N-dimethyl-formamide; at 70 - 80 ℃; for 1h;

DOI:10.1002/jhet.5570170546

Reference yield: 90.0%

Methyl 1-(2-Methanesulfonyloxyethyl)-3-methoxycarbonyl-4-(2-phenylethyl)pyrrole-2-acetate (76209-54-6) → Methyl 6-(2-Phenylethyl)-7-carbomethoxy-1,2-dihydro-3H-pyrrolo<1,2-a>pyrrole-1-carboxylate (76209-64-8)

Guidance literature:

With sodium hydride; In N,N-dimethyl-formamide; for 0.5h;

DOI:10.1002/jhet.5570170546

upstream raw materials:

Methyl 1-(2-Hydroxyethyl)-3-methoxycarbonyl-4-(2-phenylethyl)pyrrole-2-acetate

methanesulfonyl chloride

Downstream raw materials:

Methyl 6-(2-Phenylethyl)-7-carbomethoxy-1,2-dihydro-3H-pyrrolo<1,2-a>pyrrole-1-carboxylate

Methyl 1-(2-Chloroethyl)-3-methoxycarbonyl-4-(2-phenylethyl)pyrrole-2-acetate

Methyl 3-Methoxycarbonyl-4-(2-phenylethyl)pyrrole-2-acetate

Methyl 1-Vinyl-3-Methoxycarbonyl-4-(2-phenylethyl)pyrrole-2-acetate

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