1-<5'-(L-phenylalanylmethylamino)-5'-deoxy-α-L-talo-furanosyluronic acid>uracil

Base Information

Chemical Name:1-<5'-(L-phenylalanylmethylamino)-5'-deoxy-α-L-talo-furanosyluronic acid>uracil
CAS No.:100682-75-5
Molecular Formula:C₂₀H₂₄N₄O₈
Molecular Weight:448.433
Hs Code.:

Synonyms:1-<5'-(L-phenylalanylmethylamino)-5'-deoxy-α-L-talo-furanosyluronic acid>uracil

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Chemical Property of 1-<5'-(L-phenylalanylmethylamino)-5'-deoxy-α-L-talo-furanosyluronic acid>uracil

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Technology Process of 1-<5'-(L-phenylalanylmethylamino)-5'-deoxy-α-L-talo-furanosyluronic acid>uracil

There total 10 articles about 1-<5'-(L-phenylalanylmethylamino)-5'-deoxy-α-L-talo-furanosyluronic acid>uracil which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 100683-02-1
(R)-[((S)-2-Benzyloxycarbonylamino-3-phenyl-propionyl)-methyl-amino]-[(2R,3S,4R,5R)-5-(2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-3,4-dihydroxy-tetrahydro-furan-2-yl]-acetic acid

: 100682-75-5
1-<5'-(L-phenylalanylmethylamino)-5'-deoxy-α-L-talo-furanosyluronic acid>uracil

Guidance literature:: With formic acid; palladium; In methanol; for 0.5h; Heating;
DOI:10.1021/jo00362a027

Reference yield:

: 1161-13-3
N-Cbz-L-Phe

: 100682-75-5
1-<5'-(L-phenylalanylmethylamino)-5'-deoxy-α-L-talo-furanosyluronic acid>uracil

Guidance literature:: Multi-step reaction with 5 steps

1: methanol / 18 h / 25 °C

2: acetic acid / H₂O / 5 h

3: 39 percent / nitrosulfuric acid / CH₂Cl₂ / 0.5 h

4: 69 percent / 50 percent aq. HOAc / 1 h / Heating

5: 69 percent / formic acid / Pd black / methanol / 0.5 h / Heating

With formic acid; nitrosulfuric acid; acetic acid; palladium; In methanol; dichloromethane; water;
DOI:10.1021/jo00362a027

Reference yield:

: 34311-30-3
2',3'-O-cyclohexylideneuridine 5'-aldehyde

: 100682-75-5
1-<5'-(L-phenylalanylmethylamino)-5'-deoxy-α-L-talo-furanosyluronic acid>uracil

Guidance literature:: Multi-step reaction with 6 steps

1: 78 percent / 3A sieves / tetrahydrofuran / 2 h / Ambient temperature

2: methanol / 18 h / 25 °C

3: acetic acid / H₂O / 5 h

4: 39 percent / nitrosulfuric acid / CH₂Cl₂ / 0.5 h

5: 69 percent / 50 percent aq. HOAc / 1 h / Heating

6: 69 percent / formic acid / Pd black / methanol / 0.5 h / Heating

With formic acid; 3 A molecular sieve; nitrosulfuric acid; acetic acid; palladium; In tetrahydrofuran; methanol; dichloromethane; water;
DOI:10.1021/jo00362a027