Benzyl 2-acetamido-3-O-benzyl-2-deoxy-5,6-O-isopropylidene-β-D-glucofuranoside

Base Information

• Chemical Name: Benzyl 2-acetamido-3-O-benzyl-2-deoxy-5,6-O-isopropylidene-β-D-glucofuranoside
• CAS No.: 58886-35-4
• Molecular Formula: C₂₅H₃₁NO₆
• Molecular Weight: 441.524
• Mol file: 58886-35-4.mol

Synonyms:Benzyl 2-acetamido-3-O-benzyl-2-deoxy-5,6-O-isopropylidene-β-D-glucofuranoside

Chemical Property of Benzyl 2-acetamido-3-O-benzyl-2-deoxy-5,6-O-isopropylidene-β-D-glucofuranoside

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Benzyl 2-acetamido-3-O-benzyl-2-deoxy-5,6-O-isopropylidene-β-D-glucofuranoside

There total 2 articles about Benzyl 2-acetamido-3-O-benzyl-2-deoxy-5,6-O-isopropylidene-β-D-glucofuranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

2-acetamido-2-deoxy-5,6-O-isopropylidene-D-glucofuranose (86204-32-2,86204-33-3,86204-43-5,86204-46-8,117177-22-7,117177-23-8) + benzyl bromide (100-39-0) → Benzyl 2-acetamido-3-O-benzyl-2-deoxy-5,6-O-isopropylidene-β-D-glucofuranoside (58886-35-4)

Guidance literature:

With barium dihydroxide; barium(II) oxide; In N,N-dimethyl-formamide; 1) 0 deg C, 5 h, 2) r.t., 18 h;

DOI:10.1016/0008-6215(93)84048-B

Reference yield:

→ Benzyl 2-acetamido-3-O-benzyl-2-deoxy-5,6-O-isopropylidene-β-D-glucofuranoside (58886-35-4)

Guidance literature:

Alkohol 1, Benzylbromid, Ba-oxid, Ba(OH)2;

DOI:10.1016/S0008-6215(00)85862-0

Reference yield: 60.0%

Benzyl 2-acetamido-3-O-benzyl-2-deoxy-5,6-O-isopropylidene-β-D-glucofuranoside (58886-35-4) → 2-acetamido-3-O-benzyl-2-deoxy-5,6-O-isopropylidene-D-glucofuranose (125158-56-7,125158-58-9)

Guidance literature:

With ammonium formate; palladium on activated charcoal; In methanol; at 70 ℃; for 0.1h;

DOI:10.1016/0008-6215(93)84048-B

upstream raw materials:

2-acetamido-2-deoxy-5,6-O-isopropylidene-D-glucofuranose

benzyl bromide

Downstream raw materials:

2-acetamido-3-O-benzyl-2-deoxy-5,6-O-isopropylidene-D-glucofuranose

2-Acetamido-3-O-benzyl-2-deoxy-5,6-Oisopropylidene-α-D-glucofuranose

2-Acetamido-3-O-benzyl-2-deoxy-5,6-Oisopropylidene-β-D-glucofuranose