N-[4-(6-Methyl-[1,3]dioxolo[4,5-g]quinazolin-8-ylmethyl)-phenyl]-acetamide

Base Information

Chemical Name:N-[4-(6-Methyl-[1,3]dioxolo[4,5-g]quinazolin-8-ylmethyl)-phenyl]-acetamide
CAS No.:85591-04-4
Molecular Formula:C₁₉H₁₇N₃O₃
Molecular Weight:335.362
Hs Code.:

Synonyms:N-[4-(6-Methyl-[1,3]dioxolo[4,5-g]quinazolin-8-ylmethyl)-phenyl]-acetamide

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Chemical Property of N-[4-(6-Methyl-[1,3]dioxolo[4,5-g]quinazolin-8-ylmethyl)-phenyl]-acetamide

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Technology Process of N-[4-(6-Methyl-[1,3]dioxolo[4,5-g]quinazolin-8-ylmethyl)-phenyl]-acetamide

There total 6 articles about N-[4-(6-Methyl-[1,3]dioxolo[4,5-g]quinazolin-8-ylmethyl)-phenyl]-acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 38.0%

: 85590-87-0
2'-(acetylamino)-2-(4-acetylaminophenyl)-4',5'-methylenedioxyacetophenone

: 85591-04-4
N-[4-(6-Methyl-[1,3]dioxolo[4,5-g]quinazolin-8-ylmethyl)-phenyl]-acetamide

Guidance literature:: In ethanol; at 150 ℃; for 5h; Heating; sealed tube;

Reference yield:

: 274-09-9
Methylenedioxybenzene

: 85591-04-4
N-[4-(6-Methyl-[1,3]dioxolo[4,5-g]quinazolin-8-ylmethyl)-phenyl]-acetamide

Guidance literature:: Multi-step reaction with 5 steps

1: 51 percent / AlCl₃ / CH₂Cl₂ / 3 h / -35 °C

2: 92 percent / conc. HNO₃ / 0.5 h / 20 °C

3: H₂ / 8 percent Pd/C / ethyl acetate / Ambient temperature

4: CH₂Cl₂

5: 38 percent / ethanol / 5 h / 150 °C / Heating; sealed tube

With aluminium trichloride; hydrogen; nitric acid; palladium on activated charcoal; In ethanol; dichloromethane; ethyl acetate;

Reference yield:

: 85590-86-9
4',5'-methylenedioxy-2'-nitro-2-(4-nitrophenyl)acetophenone

: 85591-04-4
N-[4-(6-Methyl-[1,3]dioxolo[4,5-g]quinazolin-8-ylmethyl)-phenyl]-acetamide

Guidance literature:: Multi-step reaction with 3 steps

1: H₂ / 8 percent Pd/C / ethyl acetate / Ambient temperature

2: CH₂Cl₂

3: 38 percent / ethanol / 5 h / 150 °C / Heating; sealed tube

With hydrogen; palladium on activated charcoal; In ethanol; dichloromethane; ethyl acetate;