1,2-di-O-benzyl-3-O-[6'-O-(β-D-glucopyranosyl)-β-D-glucopyranosyl]-sn-glycerol

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Chemical Name:1,2-di-O-benzyl-3-O-[6'-O-(β-D-glucopyranosyl)-β-D-glucopyranosyl]-sn-glycerol
CAS No.:428863-07-4
Molecular Formula:C₂₉H₄₀O₁₃
Molecular Weight:596.629
Hs Code.:

Synonyms:1,2-di-O-benzyl-3-O-[6'-O-(β-D-glucopyranosyl)-β-D-glucopyranosyl]-sn-glycerol

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Chemical Property of 1,2-di-O-benzyl-3-O-[6'-O-(β-D-glucopyranosyl)-β-D-glucopyranosyl]-sn-glycerol

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Technology Process of 1,2-di-O-benzyl-3-O-[6'-O-(β-D-glucopyranosyl)-β-D-glucopyranosyl]-sn-glycerol

There total 4 articles about 1,2-di-O-benzyl-3-O-[6'-O-(β-D-glucopyranosyl)-β-D-glucopyranosyl]-sn-glycerol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 1,2-di-O-benzyl-sn-glyceryl 2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl-(1,6)-2,3,6-tri-O-benzoyl-β-D-glucopyranoside

: 428863-07-4
1,2-di-O-benzyl-3-O-[6'-O-(β-D-glucopyranosyl)-β-D-glucopyranosyl]-sn-glycerol

Guidance literature:: With methanol; sodium methylate; at 20 ℃; for 16h; Inert atmosphere;
DOI:10.1039/c5cc04773k

Reference yield: 98.0%

: 1,2-di-O-benzyl-3-O-[6'-O-(2'',3'',4'',6''-tetra-O-acetyl-β-D-glucopyranosyl)-2',3',4'-tri-O-acetyl-β-D-glucopyranosyl]-sn-glycerol

: 428863-07-4
1,2-di-O-benzyl-3-O-[6'-O-(β-D-glucopyranosyl)-β-D-glucopyranosyl]-sn-glycerol

Guidance literature:: With methanol; sodium methylate; at 20 ℃; pH=8 - 9;
DOI:10.1016/S0009-3084(01)00202-X

Reference yield:

: 20196-71-8
(2S)-2,3-bis(benzyloxy)propanol

: 428863-07-4
1,2-di-O-benzyl-3-O-[6'-O-(β-D-glucopyranosyl)-β-D-glucopyranosyl]-sn-glycerol

Guidance literature:: Multi-step reaction with 2 steps

1: 71 percent / BF₃*Et₂O / CH₂Cl₂ / 20 °C

2: 98 percent / NaOMe; MeOH / 20 °C / pH 8 - 9

With methanol; boron trifluoride diethyl etherate; sodium methylate; In dichloromethane;
DOI:10.1016/S0009-3084(01)00202-X