1,4-bis[2-(2-(2-hydroxyethoxy)ethoxy)ethoxy]benzene monotosylate

Base Information

Chemical Name:1,4-bis[2-(2-(2-hydroxyethoxy)ethoxy)ethoxy]benzene monotosylate
CAS No.:224298-61-7
Molecular Formula:C₂₅H₃₆O₁₀S
Molecular Weight:528.621
Hs Code.:

Synonyms:1,4-bis[2-(2-(2-hydroxyethoxy)ethoxy)ethoxy]benzene monotosylate

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Chemical Property of 1,4-bis[2-(2-(2-hydroxyethoxy)ethoxy)ethoxy]benzene monotosylate

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Technology Process of 1,4-bis[2-(2-(2-hydroxyethoxy)ethoxy)ethoxy]benzene monotosylate

There total 3 articles about 1,4-bis[2-(2-(2-hydroxyethoxy)ethoxy)ethoxy]benzene monotosylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

: 134881-72-4
1,4-bis-(2-(2-(2-hydroxyethoxy)ethoxy)ethoxy)benzene

: 98-59-9
p-toluenesulfonyl chloride

: 224298-61-7
1,4-bis[2-(2-(2-hydroxyethoxy)ethoxy)ethoxy]benzene monotosylate

Guidance literature:: 1,4-bis-(2-(2-(2-hydroxyethoxy)ethoxy)ethoxy)benzene; With sodium hydroxide; In tetrahydrofuran; water; at 20 ℃;

p-toluenesulfonyl chloride; In tetrahydrofuran; at 20 ℃; for 24h;
DOI:10.1021/acs.inorgchem.0c00735

Reference yield:

: 123-31-9,8027-02-9
hydroquinone

: 224298-61-7
1,4-bis[2-(2-(2-hydroxyethoxy)ethoxy)ethoxy]benzene monotosylate

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium carbonate / acetonitrile / 72 h / 130 °C / Sealed tube; High pressure

2.1: sodium hydroxide / tetrahydrofuran; water / 20 °C

2.2: 24 h / 20 °C

With potassium carbonate; sodium hydroxide; In tetrahydrofuran; water; acetonitrile;
DOI:10.1021/acs.inorgchem.0c00735

Reference yield:

: 5197-62-6
2-[2-(chloroethoxy)ethoxy]ethanol

: 224298-61-7
1,4-bis[2-(2-(2-hydroxyethoxy)ethoxy)ethoxy]benzene monotosylate

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium carbonate / acetonitrile / 72 h / 130 °C / Sealed tube; High pressure

2.1: sodium hydroxide / tetrahydrofuran; water / 20 °C

2.2: 24 h / 20 °C

With potassium carbonate; sodium hydroxide; In tetrahydrofuran; water; acetonitrile;
DOI:10.1021/acs.inorgchem.0c00735