cyclopentyl (2S)-[(4-{[(tert-butoxycarbonyl)amino]methyl}benzyl)amino](cyclohexyl)acetate

Base Information

Chemical Name:cyclopentyl (2S)-[(4-{[(tert-butoxycarbonyl)amino]methyl}benzyl)amino](cyclohexyl)acetate
CAS No.:1018674-41-3
Molecular Formula:C₂₆H₄₀N₂O₄
Molecular Weight:444.615
Hs Code.:

Synonyms:cyclopentyl (2S)-[(4-{[(tert-butoxycarbonyl)amino]methyl}benzyl)amino](cyclohexyl)acetate

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Chemical Property of cyclopentyl (2S)-[(4-{[(tert-butoxycarbonyl)amino]methyl}benzyl)amino](cyclohexyl)acetate

Chemical Property:

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Technology Process of cyclopentyl (2S)-[(4-{[(tert-butoxycarbonyl)amino]methyl}benzyl)amino](cyclohexyl)acetate

There total 7 articles about cyclopentyl (2S)-[(4-{[(tert-butoxycarbonyl)amino]methyl}benzyl)amino](cyclohexyl)acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 956928-36-2
cyclopentyl (2S)-amino(cyclohexyl)acetate hydrochloride

: 156866-52-3
tert-butyl N-(4-formylbenzyl)carbamate

: 1018674-41-3
cyclopentyl (2S)-[(4-{[(tert-butoxycarbonyl)amino]methyl}benzyl)amino](cyclohexyl)acetate

Guidance literature:: With sodium tris(acetoxy)borohydride; In 1,2-dichloro-ethane; at 20 ℃; for 3h;

Reference yield:

: 914604-31-2
(S)-tert-butoxycarbonylamino-cyclohexyl-acetic acid cyclopentyl ester

: 1018674-41-3
cyclopentyl (2S)-[(4-{[(tert-butoxycarbonyl)amino]methyl}benzyl)amino](cyclohexyl)acetate

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogenchloride / 1,4-dioxane; dichloromethane / 24 h / 20 °C

2: sodium tris(acetoxy)borohydride / 1,2-dichloro-ethane / 3 h / 20 °C

With hydrogenchloride; sodium tris(acetoxy)borohydride; In 1,4-dioxane; dichloromethane; 1,2-dichloro-ethane;

Reference yield:

: 56-91-7
p-aminomethylbenzoic acid

: 1018674-41-3
cyclopentyl (2S)-[(4-{[(tert-butoxycarbonyl)amino]methyl}benzyl)amino](cyclohexyl)acetate

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium hydrogencarbonate / tetrahydrofuran; water / 16 h / 20 °C / pH 6

1.2: pH 3

2.1: lithium aluminium tetrahydride / tetrahydrofuran; 1,4-dioxane / 16 h / 0 - 20 °C

2.2: 0.5 h / 0 °C

3.1: manganese(IV) oxide / dichloromethane / 16 h / 20 °C

4.1: sodium tris(acetoxy)borohydride / 1,2-dichloro-ethane / 3 h / 20 °C

With manganese(IV) oxide; lithium aluminium tetrahydride; sodium tris(acetoxy)borohydride; sodium hydrogencarbonate; In tetrahydrofuran; 1,4-dioxane; dichloromethane; water; 1,2-dichloro-ethane;