(4-amino-4-cyanocyclohexane-1,1-diyl)bis(methylene)bis(4-methylbenzenesulfonate)

Base Information

Chemical Name:(4-amino-4-cyanocyclohexane-1,1-diyl)bis(methylene)bis(4-methylbenzenesulfonate)
CAS No.:1380664-91-4
Molecular Formula:C₂₃H₂₈N₂O₆S₂
Molecular Weight:492.617
Hs Code.:

Synonyms:(4-amino-4-cyanocyclohexane-1,1-diyl)bis(methylene)bis(4-methylbenzenesulfonate)

Suppliers and Price of (4-amino-4-cyanocyclohexane-1,1-diyl)bis(methylene)bis(4-methylbenzenesulfonate)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (4-amino-4-cyanocyclohexane-1,1-diyl)bis(methylene)bis(4-methylbenzenesulfonate)

Chemical Property:

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Technology Process of (4-amino-4-cyanocyclohexane-1,1-diyl)bis(methylene)bis(4-methylbenzenesulfonate)

There total 8 articles about (4-amino-4-cyanocyclohexane-1,1-diyl)bis(methylene)bis(4-methylbenzenesulfonate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 773837-37-9
sodium cyanide

: 340022-81-3
(4-oxocyclohexane-1,1-diyl)bis(methylene) bis(4-methylbenzenesulfonate)

: 1380664-91-4
(4-amino-4-cyanocyclohexane-1,1-diyl)bis(methylene)bis(4-methylbenzenesulfonate)

Guidance literature:: (4-oxocyclohexane-1,1-diyl)bis(methylene) bis(4-methylbenzenesulfonate); With ammonium hydroxide; ammonium chloride; In tetrahydrofuran; methanol;

sodium cyanide; In tetrahydrofuran; methanol;

Reference yield:

: 55704-60-4
4-oxo-cyclohexane-1,1-dicarboxylic acid diethyl ester

: 1380664-91-4
(4-amino-4-cyanocyclohexane-1,1-diyl)bis(methylene)bis(4-methylbenzenesulfonate)

Guidance literature:: Multi-step reaction with 5 steps

1.1: toluene-4-sulfonic acid / benzene / 48 h / 20 °C / Inert atmosphere

2.1: lithium aluminium tetrahydride / tetrahydrofuran / 10 - 20 °C / Inert atmosphere; Cooling with acetone-dry ice

2.2: 1.5 h / -5 - 30 °C

3.1: pyridine / dmap / 48 h / 20 °C

4.1: hydrogenchloride; water / tetrahydrofuran / 3.5 h / 52 °C

5.1: ammonium hydroxide; ammonium chloride / tetrahydrofuran; methanol

With pyridine; hydrogenchloride; ammonium hydroxide; lithium aluminium tetrahydride; water; ammonium chloride; dmap; toluene-4-sulfonic acid; In tetrahydrofuran; methanol; benzene;

Reference yield:

: 1,5-di-tert-butyl 3,3-diethyl pentane-1,3,3,5-tetracarboxylate

: 1380664-91-4
(4-amino-4-cyanocyclohexane-1,1-diyl)bis(methylene)bis(4-methylbenzenesulfonate)

Guidance literature:: Multi-step reaction with 7 steps

1.1: trifluoroacetic acid / dichloromethane / 36 h

2.1: acetic anhydride; pyridine / 3 h / Reflux

2.2: 16 h

3.1: toluene-4-sulfonic acid / benzene / 48 h / 20 °C / Inert atmosphere

4.1: lithium aluminium tetrahydride / tetrahydrofuran / 10 - 20 °C / Inert atmosphere; Cooling with acetone-dry ice

4.2: 1.5 h / -5 - 30 °C

5.1: pyridine / dmap / 48 h / 20 °C

6.1: hydrogenchloride; water / tetrahydrofuran / 3.5 h / 52 °C

7.1: ammonium hydroxide; ammonium chloride / tetrahydrofuran; methanol

With pyridine; hydrogenchloride; ammonium hydroxide; lithium aluminium tetrahydride; water; acetic anhydride; ammonium chloride; trifluoroacetic acid; dmap; toluene-4-sulfonic acid; In tetrahydrofuran; methanol; dichloromethane; benzene;