[1-13C]GLYCOLALDEHYDE

Base Information

• Chemical Name: [1-13C]GLYCOLALDEHYDE
• CAS No.: 71122-42-4
• Molecular Formula: C₂H₄O₂
• Molecular Weight: 61.0416
• Mol file: 71122-42-4.mol

Synonyms:[1-13C]GLYCOLALDEHYDE

Chemical Property of [1-13C]GLYCOLALDEHYDE

Chemical Property:

• PSA: 37.30000
• LogP: -0.82240
• Storage Temp.: Refrigerator, under inert atmosphere
• Solubility.: DMSO (Soluble), Methanol (Slightly)

Purity/Quality:

99% ^*data from raw suppliers

Glycolaldehyde-1-13C(5mg/mLinwater) ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of [1-13C]GLYCOLALDEHYDE

There total 3 articles about [1-13C]GLYCOLALDEHYDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

formaldehyd (50-00-0,30525-89-4,61233-19-0) + [13C]-potassium cyanide (25909-68-6) → [1-13C]-glycolaldehyde (71122-42-4)

Guidance literature:

With Pd-BaSO₄; hydrogen; 2) 1 atm, pH 1.7;

DOI:10.1021/jo00167a012

Reference yield:

formaldehyd (50-00-0,30525-89-4,61233-19-0) + potassium [13C]cyanide → [1-13C]-glycolaldehyde (71122-42-4)

Guidance literature:

With hydrogen; Pd-BaSO₄; Yield given. Multistep reaction; 1.) pH 7.2-7.5;

DOI:10.1021/ja00246a001

Reference yield:

→ [1-13C]-glycolaldehyde (71122-42-4)

Guidance literature:

Formaldehyd 1. K¹³CN 2. H2, Pd/BaSO4;

DOI:10.1016/S0008-6215(00)83925-7

upstream raw materials:

formaldehyd

[¹³C]-potassium cyanide

Downstream raw materials:

[2-13C]-DL-glyceraldehyde

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