(1r,4r)-6'-bromo-4-methoxyspiro[cyclohexane-1,2'-inden]-1'(3'H)-imine hydrochloride

Base Information

Chemical Name:(1r,4r)-6'-bromo-4-methoxyspiro[cyclohexane-1,2'-inden]-1'(3'H)-imine hydrochloride
CAS No.:1383985-61-2
Molecular Formula:C₁₅H₁₈BrNO*ClH
Molecular Weight:344.679
Hs Code.:
Mol file:1383985-61-2.mol

Synonyms:(1r,4r)-6'-bromo-4-methoxyspiro[cyclohexane-1,2'-inden]-1'(3'H)-imine hydrochloride

Suppliers and Price of (1r,4r)-6'-bromo-4-methoxyspiro[cyclohexane-1,2'-inden]-1'(3'H)-imine hydrochloride

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemicals and raw materials
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price

Total 2 raw suppliers

Chemical Property of (1r,4r)-6'-bromo-4-methoxyspiro[cyclohexane-1,2'-inden]-1'(3'H)-imine hydrochloride

Chemical Property:

Purity/Quality:: 97% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

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Technology Process of (1r,4r)-6'-bromo-4-methoxyspiro[cyclohexane-1,2'-inden]-1'(3'H)-imine hydrochloride

There total 13 articles about (1r,4r)-6'-bromo-4-methoxyspiro[cyclohexane-1,2'-inden]-1'(3'H)-imine hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 1245516-72-6
(1r,4r)-6’-bromo-4-methoxyspiro(cyclohexane-1,2’-indene)-1’(3’H)-one

: 1383985-61-2
(1r,4r)-6'-bromo-4-methoxyspiro[cyclohexane-1,2'-inden]-1'(3'H)-imine hydrochloride

Guidance literature:: With titanium(IV) isopropylate; ammonia; In methanol; at 120 ℃; for 0.25h; Concentration; Solvent; Temperature; Time; Reagent/catalyst; Sealed tube;
DOI:10.1021/acs.oprd.8b00089

Reference yield: 92.0%

: 1383985-60-1
N-((1r,4r)-5'-bromo-4-methoxyspiro[cyclohexane-1,2'-indene]-3'(1'H)-ylidene)-2-methylpropane-2-sulfinamide

: 1383985-61-2
(1r,4r)-6'-bromo-4-methoxyspiro[cyclohexane-1,2'-inden]-1'(3'H)-imine hydrochloride

Guidance literature:: With hydrogenchloride; In diethyl ether; dichloromethane; for 1h; Time; Temperature;

Reference yield: 79.0%

: 1245516-72-6
(1r,4r)-6’-bromo-4-methoxyspiro(cyclohexane-1,2’-indene)-1’(3’H)-one

: 146374-27-8
S-tert-butylsulfinimide

: 1383985-61-2
(1r,4r)-6'-bromo-4-methoxyspiro[cyclohexane-1,2'-inden]-1'(3'H)-imine hydrochloride

Guidance literature:: (1r,4r)-6’-bromo-4-methoxyspiro(cyclohexane-1,2’-indene)-1’(3’H)-one; S-tert-butylsulfinimide; With titanium(IV) tetraethanolate; In 2-methyltetrahydrofuran; at 82 ℃; for 17.5h;

With hydrogenchloride; In ethanol; dichloromethane; at 20 ℃; for 1.08333h;