1-({[tert-butyl(dimethyl)silyl]oxy}methyl)-4-isopropyl-2,3,5-trimethoxybenzene

Base Information

Chemical Name:1-({[tert-butyl(dimethyl)silyl]oxy}methyl)-4-isopropyl-2,3,5-trimethoxybenzene
CAS No.:914618-43-2
Molecular Formula:C₁₉H₃₄O₄Si
Molecular Weight:354.562
Hs Code.:

Synonyms:1-({[tert-butyl(dimethyl)silyl]oxy}methyl)-4-isopropyl-2,3,5-trimethoxybenzene

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Chemical Property of 1-({[tert-butyl(dimethyl)silyl]oxy}methyl)-4-isopropyl-2,3,5-trimethoxybenzene

Chemical Property:

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Technology Process of 1-({[tert-butyl(dimethyl)silyl]oxy}methyl)-4-isopropyl-2,3,5-trimethoxybenzene

There total 3 articles about 1-({[tert-butyl(dimethyl)silyl]oxy}methyl)-4-isopropyl-2,3,5-trimethoxybenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 69739-34-0
t-butyldimethylsiyl triflate

: 156723-06-7
4-(1-methylethyl)-2,3,5-trimethoxyphenylmethyl alcohol

: 914618-43-2
1-({[tert-butyl(dimethyl)silyl]oxy}methyl)-4-isopropyl-2,3,5-trimethoxybenzene

Guidance literature:: With 2,6-dimethylpyridine; In dichloromethane; at 0 - 20 ℃;
DOI:10.1002/ejoc.200600361

Reference yield:

: 914618-38-5
6-(hydroxymethyl)-3-isopropyl-2,4-dimethoxyphenol

: 914618-43-2
1-({[tert-butyl(dimethyl)silyl]oxy}methyl)-4-isopropyl-2,3,5-trimethoxybenzene

Guidance literature:: Multi-step reaction with 2 steps

1: 99 percent / potassium carbonate / acetone / 6 h / Heating

2: 99 percent / 2,6-lutidine / CH₂Cl₂ / 0 - 20 °C

With 2,6-dimethylpyridine; potassium carbonate; In dichloromethane; acetone;
DOI:10.1002/ejoc.200600361

Reference yield:

: 144707-39-1
1,3-Dimethoxy-4-hydroxy-2-isopropylbenzene

: 914618-43-2
1-({[tert-butyl(dimethyl)silyl]oxy}methyl)-4-isopropyl-2,3,5-trimethoxybenzene

Guidance literature:: Multi-step reaction with 3 steps

1: 99 percent / diethylaluminum chloride / CH₂Cl₂; hexane / 0 - 20 °C

2: 99 percent / potassium carbonate / acetone / 6 h / Heating

3: 99 percent / 2,6-lutidine / CH₂Cl₂ / 0 - 20 °C

With 2,6-dimethylpyridine; diethylaluminium chloride; potassium carbonate; In hexane; dichloromethane; acetone;
DOI:10.1002/ejoc.200600361