2-phenyl>-3,3,5-trimethyloxazolidinium iodide

Base Information

Chemical Name:2-phenyl>-3,3,5-trimethyloxazolidinium iodide
CAS No.:84694-33-7
Molecular Formula:C₁₆H₂₈NOSi*I
Molecular Weight:405.394
Hs Code.:

2-<o-<(trimethylsilyl)methyl>phenyl>-3,3,5-trimethyloxazolidinium iodide

Synonyms:2-phenyl>-3,3,5-trimethyloxazolidinium iodide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-phenyl>-3,3,5-trimethyloxazolidinium iodide

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Technology Process of 2-phenyl>-3,3,5-trimethyloxazolidinium iodide

There total 3 articles about 2-phenyl>-3,3,5-trimethyloxazolidinium iodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 84694-22-4
2-phenyl>-3,5-dimethyloxazolidine

: 74-88-4
methyl iodide

: 84694-33-7
2-phenyl>-3,3,5-trimethyloxazolidinium iodide

Guidance literature:: In acetonitrile; at 40 - 50 ℃; for 7h;
DOI:10.1021/ja00344a028

Reference yield:

: 84694-17-7
2-phenyl>-5-methyloxazoline

: 84694-33-7
2-phenyl>-3,3,5-trimethyloxazolidinium iodide

Guidance literature:: Multi-step reaction with 3 steps

1: acetonitrile / 7 h / 40 - 50 °C

2: NaBH₄ / methanol / 0.08 h / -78 °C

3: 90 percent / acetonitrile / 7 h / 40 - 50 °C

With sodium tetrahydroborate; In methanol; acetonitrile;
DOI:10.1021/ja00344a028

Reference yield:

: 3,5-Dimethyl-2-(2-trimethylsilanylmethyl-phenyl)-4,5-dihydro-oxazol-3-ium; iodide

: 84694-33-7
2-phenyl>-3,3,5-trimethyloxazolidinium iodide

Guidance literature:: Multi-step reaction with 2 steps

1: NaBH₄ / methanol / 0.08 h / -78 °C

2: 90 percent / acetonitrile / 7 h / 40 - 50 °C

With sodium tetrahydroborate; In methanol; acetonitrile;
DOI:10.1021/ja00344a028