(S)-2-amino-N-((S)-1-amino-3-(4-t-butoxyphenyl)-1-oxopropan-2-yl)propanamide

Base Information

Chemical Name:(S)-2-amino-N-((S)-1-amino-3-(4-t-butoxyphenyl)-1-oxopropan-2-yl)propanamide
CAS No.:1082954-31-1
Molecular Formula:C₁₆H₂₅N₃O₃
Molecular Weight:307.393
Hs Code.:

Synonyms:(S)-2-amino-N-((S)-1-amino-3-(4-t-butoxyphenyl)-1-oxopropan-2-yl)propanamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-2-amino-N-((S)-1-amino-3-(4-t-butoxyphenyl)-1-oxopropan-2-yl)propanamide

Chemical Property:

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Technology Process of (S)-2-amino-N-((S)-1-amino-3-(4-t-butoxyphenyl)-1-oxopropan-2-yl)propanamide

There total 3 articles about (S)-2-amino-N-((S)-1-amino-3-(4-t-butoxyphenyl)-1-oxopropan-2-yl)propanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1194838-69-1
C₂₄H₃₁N₃O₅

: 1082954-31-1
(S)-2-amino-N-((S)-1-amino-3-(4-t-butoxyphenyl)-1-oxopropan-2-yl)propanamide

Guidance literature:: With palladium 10% on activated carbon; hydrogen; In ethanol; N,N-dimethyl-formamide; for 2h; Inert atmosphere;
DOI:10.1021/jm8004515

Reference yield:

: 39894-76-3
(S)-benzyl-1-amino-3-(4-t-butoxyphenyl)-1-oxopropan-2-ylcarbamate

: 1082954-31-1
(S)-2-amino-N-((S)-1-amino-3-(4-t-butoxyphenyl)-1-oxopropan-2-yl)propanamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: hydrogen / palladium 10% on activated carbon / ethanol / 3 h / Inert atmosphere

2.1: 1,1'-carbonyldiimidazole / tetrahydrofuran / 2 h / Inert atmosphere

2.2: 48 h / Inert atmosphere

3.1: hydrogen / palladium 10% on activated carbon / ethanol / 20 h / Inert atmosphere

With hydrogen; 1,1'-carbonyldiimidazole; palladium 10% on activated carbon; In tetrahydrofuran; ethanol;

Reference yield:

: 16879-90-6,198828-72-7
N-α-benzyloxycarbamoyl-O-t-butyl-L-tyrosine dicyclohexylammonium salt

: 1082954-31-1
(S)-2-amino-N-((S)-1-amino-3-(4-t-butoxyphenyl)-1-oxopropan-2-yl)propanamide

Guidance literature:: Multi-step reaction with 4 steps

1.1: 4-methyl-morpholine; isobutyl chloroformate / tetrahydrofuran; 1,2-dimethoxyethane / 1 h / Cooling with ice; Inert atmosphere

1.2: 0.5 h / Inert atmosphere

2.1: hydrogen / palladium 10% on activated carbon / ethanol / 3 h / Inert atmosphere

3.1: 1,1'-carbonyldiimidazole / tetrahydrofuran / 2 h / Inert atmosphere

3.2: 48 h / Inert atmosphere

4.1: hydrogen / palladium 10% on activated carbon / ethanol / 20 h / Inert atmosphere

With 4-methyl-morpholine; hydrogen; 1,1'-carbonyldiimidazole; isobutyl chloroformate; palladium 10% on activated carbon; In tetrahydrofuran; 1,2-dimethoxyethane; ethanol;