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C30H41N5O2Si

Base Information
  • Chemical Name:C30H41N5O2Si
  • CAS No.:1276126-12-5
  • Molecular Formula:C30H41N5O2Si
  • Molecular Weight:531.773
  • Hs Code.:
C<sub>30</sub>H<sub>41</sub>N<sub>5</sub>O<sub>2</sub>Si

Synonyms:C30H41N5O2Si

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Chemical Property of C30H41N5O2Si
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Technology Process of C30H41N5O2Si

There total 14 articles about C30H41N5O2Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
With 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; sodium t-butanolate; tris-(dibenzylideneacetone)dipalladium(0); In toluene; at 105 ℃; for 6h; Inert atmosphere;
Guidance literature:
Multi-step reaction with 7 steps
1.1: triethylamine / dichloromethane / 3 h / Inert atmosphere; Cooling with ice bath
2.1: sodium hydride / tetrahydrofuran / 20 °C / Inert atmosphere
2.2: pH 3 / Ice water
3.1: hydrazine dihydrochloride / ethanol / 2.5 h / 60 °C
4.1: sodium hydride / tetrahydrofuran; mineral oil / 0.33 h / 0 °C
4.2: 20 °C
5.1: hydrogen / palladium 10% on activated carbon / ethanol / 6 h / 20 °C / 760.05 Torr
6.1: N-ethyl-N,N-diisopropylamine; HATU / N,N-dimethyl-formamide / 1 h / 20 °C
6.2: 25 - 70 °C
7.1: 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; sodium t-butanolate / tris-(dibenzylideneacetone)dipalladium(0) / toluene / 6 h / 105 °C / Inert atmosphere
With hydrazine dihydrochloride; hydrogen; sodium hydride; triethylamine; N-ethyl-N,N-diisopropylamine; HATU; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; sodium t-butanolate; tris-(dibenzylideneacetone)dipalladium(0); palladium 10% on activated carbon; In tetrahydrofuran; ethanol; dichloromethane; N,N-dimethyl-formamide; toluene; mineral oil;
Guidance literature:
Multi-step reaction with 6 steps
1.1: sodium hydride / tetrahydrofuran / 20 °C / Inert atmosphere
1.2: pH 3 / Ice water
2.1: hydrazine dihydrochloride / ethanol / 2.5 h / 60 °C
3.1: sodium hydride / tetrahydrofuran; mineral oil / 0.33 h / 0 °C
3.2: 20 °C
4.1: hydrogen / palladium 10% on activated carbon / ethanol / 6 h / 20 °C / 760.05 Torr
5.1: N-ethyl-N,N-diisopropylamine; HATU / N,N-dimethyl-formamide / 1 h / 20 °C
5.2: 25 - 70 °C
6.1: 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; sodium t-butanolate / tris-(dibenzylideneacetone)dipalladium(0) / toluene / 6 h / 105 °C / Inert atmosphere
With hydrazine dihydrochloride; hydrogen; sodium hydride; N-ethyl-N,N-diisopropylamine; HATU; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; sodium t-butanolate; tris-(dibenzylideneacetone)dipalladium(0); palladium 10% on activated carbon; In tetrahydrofuran; ethanol; N,N-dimethyl-formamide; toluene; mineral oil;
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