Technology Process of C30H41N5O2Si
There total 14 articles about C30H41N5O2Si which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; sodium t-butanolate;
tris-(dibenzylideneacetone)dipalladium(0);
In
toluene;
at 105 ℃;
for 6h;
Inert atmosphere;
- Guidance literature:
-
Multi-step reaction with 7 steps
1.1: triethylamine / dichloromethane / 3 h / Inert atmosphere; Cooling with ice bath
2.1: sodium hydride / tetrahydrofuran / 20 °C / Inert atmosphere
2.2: pH 3 / Ice water
3.1: hydrazine dihydrochloride / ethanol / 2.5 h / 60 °C
4.1: sodium hydride / tetrahydrofuran; mineral oil / 0.33 h / 0 °C
4.2: 20 °C
5.1: hydrogen / palladium 10% on activated carbon / ethanol / 6 h / 20 °C / 760.05 Torr
6.1: N-ethyl-N,N-diisopropylamine; HATU / N,N-dimethyl-formamide / 1 h / 20 °C
6.2: 25 - 70 °C
7.1: 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; sodium t-butanolate / tris-(dibenzylideneacetone)dipalladium(0) / toluene / 6 h / 105 °C / Inert atmosphere
With
hydrazine dihydrochloride; hydrogen; sodium hydride; triethylamine; N-ethyl-N,N-diisopropylamine; HATU; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; sodium t-butanolate;
tris-(dibenzylideneacetone)dipalladium(0); palladium 10% on activated carbon;
In
tetrahydrofuran; ethanol; dichloromethane; N,N-dimethyl-formamide; toluene; mineral oil;
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: sodium hydride / tetrahydrofuran / 20 °C / Inert atmosphere
1.2: pH 3 / Ice water
2.1: hydrazine dihydrochloride / ethanol / 2.5 h / 60 °C
3.1: sodium hydride / tetrahydrofuran; mineral oil / 0.33 h / 0 °C
3.2: 20 °C
4.1: hydrogen / palladium 10% on activated carbon / ethanol / 6 h / 20 °C / 760.05 Torr
5.1: N-ethyl-N,N-diisopropylamine; HATU / N,N-dimethyl-formamide / 1 h / 20 °C
5.2: 25 - 70 °C
6.1: 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; sodium t-butanolate / tris-(dibenzylideneacetone)dipalladium(0) / toluene / 6 h / 105 °C / Inert atmosphere
With
hydrazine dihydrochloride; hydrogen; sodium hydride; N-ethyl-N,N-diisopropylamine; HATU; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; sodium t-butanolate;
tris-(dibenzylideneacetone)dipalladium(0); palladium 10% on activated carbon;
In
tetrahydrofuran; ethanol; N,N-dimethyl-formamide; toluene; mineral oil;