1,2-di-O-oleoyl-sn-glycero-3-phospho-(2,4-dichlorophenol) triethylammonium salt

Base Information

• Chemical Name: 1,2-di-O-oleoyl-sn-glycero-3-phospho-(2,4-dichlorophenol) triethylammonium salt
• CAS No.: 102916-98-3
• Molecular Formula: C₆H₁₅N*C₄₅H₇₅Cl₂O₈P
• Molecular Weight: 947.157
• Mol file: 102916-98-3.mol

Synonyms:1,2-di-O-oleoyl-sn-glycero-3-phospho-(2,4-dichlorophenol) triethylammonium salt

Chemical Property of 1,2-di-O-oleoyl-sn-glycero-3-phospho-(2,4-dichlorophenol) triethylammonium salt

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1,2-di-O-oleoyl-sn-glycero-3-phospho-(2,4-dichlorophenol) triethylammonium salt

There total 3 articles about 1,2-di-O-oleoyl-sn-glycero-3-phospho-(2,4-dichlorophenol) triethylammonium salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2,4-dichlorophenylphosphorodichloridate (19430-75-2) → (Z)-Octadec-9-enoic acid 2-[(2,4-dichloro-phenoxy)-hydroxy-phosphoryloxy]-1-((Z)-octadec-9-enoyloxymethyl)-ethyl ester; compound with triethyl-amine (102916-98-3)

Guidance literature:

Multi-step reaction with 2 steps

1: triethylamine / tetrahydrofuran / 0.25 h / 20 °C

2: 1.22 mmol / H₂O / tetrahydrofuran; pyridine

With water; triethylamine; In tetrahydrofuran; pyridine;

DOI:10.1016/S0040-4039(00)78751-X

Reference yield:

1,2-dioleyl-3-triphenylmethyl-sn-glycerol (69256-20-8) → (Z)-Octadec-9-enoic acid 2-[(2,4-dichloro-phenoxy)-hydroxy-phosphoryloxy]-1-((Z)-octadec-9-enoyloxymethyl)-ethyl ester; compound with triethyl-amine (102916-98-3)

Guidance literature:

Multi-step reaction with 2 steps

1: silicic acid / boric acid

2: 1.22 mmol / H₂O / tetrahydrofuran; pyridine

With water; boric acid; silicic acid; In tetrahydrofuran; pyridine;

DOI:10.1016/S0040-4039(00)78751-X

Reference yield:

1,2-dioleoylglycerol (2442-61-7,3738-74-7,22202-42-2,24529-88-2,26540-69-2,33735-55-6,38738-56-6,98719-67-6) + 2,4-dichlorophenylphosphoditriazolide (76679-70-4) → (Z)-Octadec-9-enoic acid 2-[(2,4-dichloro-phenoxy)-hydroxy-phosphoryloxy]-1-((Z)-octadec-9-enoyloxymethyl)-ethyl ester; compound with triethyl-amine (102916-98-3)

Guidance literature:

With water; In tetrahydrofuran; pyridine;

DOI:10.1016/S0040-4039(00)78751-X

upstream raw materials:

1,2-dioleoylglycerol

2,4-dichlorophenylphosphoditriazolide

2,4-dichlorophenylphosphorodichloridate

1,2-dioleyl-3-triphenylmethyl-sn-glycerol

Downstream raw materials:

C₉₈H₁₇₇Cl₂O₁₈PSi₂

C₁₃₂H₂₁₁Cl₂O₂₃PSi₂

C₉₈H₁₇₇Cl₂O₁₈PSi₂