N-diphenyl-N-pinacolborylaniline

Base Information

• Chemical Name: N-diphenyl-N-pinacolborylaniline
• CAS No.: 1426958-28-2
• Molecular Formula: C₂₅H₂₈BNO₂
• Molecular Weight: 385.314
• Mol file: 1426958-28-2.mol

Synonyms:N-diphenyl-N-pinacolborylaniline

Chemical Property of N-diphenyl-N-pinacolborylaniline

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N-diphenyl-N-pinacolborylaniline

There total 3 articles about N-diphenyl-N-pinacolborylaniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-(diphenylmethylidene)phenylamine (574-45-8) + 4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane (25015-63-8) → N-diphenyl-N-pinacolborylaniline (1426958-28-2)

Guidance literature:

With [HC{(Me)CN(2,6-ⁱPr₂C₆H₃)}₂MgⁿBu]; In benzene-d6; at 70 ℃; for 96h; Inert atmosphere;

DOI:10.1002/chem.201203190

Reference yield:

benzophenone (119-61-9) → N-diphenyl-N-pinacolborylaniline (1426958-28-2)

Guidance literature:

Multi-step reaction with 2 steps

1: dichloromethane / 18 h / 20 °C / Inert atmosphere; Molecular sieve

2: [HC{(Me)CN(2,6-ⁱPr₂C₆H₃)}₂MgⁿBu] / benzene-d6 / 96 h / 70 °C / Inert atmosphere

With [HC{(Me)CN(2,6-ⁱPr₂C₆H₃)}₂MgⁿBu]; In dichloromethane; benzene-d6;

DOI:10.1002/chem.201203190

Reference yield:

aniline (62-53-3) → N-diphenyl-N-pinacolborylaniline (1426958-28-2)

Guidance literature:

Multi-step reaction with 2 steps

1: dichloromethane / 18 h / 20 °C / Inert atmosphere; Molecular sieve

2: [HC{(Me)CN(2,6-ⁱPr₂C₆H₃)}₂MgⁿBu] / benzene-d6 / 96 h / 70 °C / Inert atmosphere

With [HC{(Me)CN(2,6-ⁱPr₂C₆H₃)}₂MgⁿBu]; In dichloromethane; benzene-d6;

DOI:10.1002/chem.201203190

upstream raw materials:

N-(diphenylmethylidene)phenylamine

4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane

aniline

benzophenone

Downstream raw materials:

N-(diphenylmethyl)aniline