Pd2I2(μ-bis(diphenylphosphino)methane)2

Base Information

Chemical Name:Pd2I2(μ-bis(diphenylphosphino)methane)2
CAS No.:67477-87-6
Molecular Formula:C₅₀H₄₄I₂P₄Pd₂
Molecular Weight:1235.44
Hs Code.:

Synonyms:Pd2I2(μ-bis(diphenylphosphino)methane)2

Suppliers and Price of Pd2I2(μ-bis(diphenylphosphino)methane)2

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Pd2I2(μ-bis(diphenylphosphino)methane)2

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of Pd2I2(μ-bis(diphenylphosphino)methane)2

There total 8 articles about Pd2I2(μ-bis(diphenylphosphino)methane)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: Pd₂(bis(diphenylphosphino)methane)3

: 77462-40-9
PdI₂(bis(diphenylphosphino)methane)

: 67477-87-6
Pd2I2(μ-dpm)2

Guidance literature:: In dichloromethane; Pd-complexes were dissolved in CH2Cl2, allowed to stand for 2 h; filtered, ether was added;

Reference yield: 29.0%

: 110981-64-1
FeI₂(CO)((C₆H₅)2PCH₂P(C₆H₅)2)2

: 32005-36-0
bis(dibenzylideneacetone)-palladium⁽⁰⁾

: 67477-87-6
Pd2I2(μ-dpm)2

: 110981-66-3
IFe(CO)2((C₆H₅)2PCH₂P(C₆H₅)2)2PdI

Guidance literature:: With carbon monoxide; In benzene; Pd- and Fe-complexes were stirred together in benzene with CO bubbling through the soln. for 3 h; filtered, excess of Et2O was added to the filtrate, mixt. was refrigerated (5°C) overnight, in cases when crystals of heterobimetallic complex were contaminated with Pd2-compound (identified by (31)P NMR), mixt. was sepd. manually; elem. anal.;
DOI:10.1039/DT9870002005