1-Methoxy-2-((S)-2-methoxy-1-methyl-ethyl)-4-[(E)-2-((S)-2,6,6-trimethyl-cyclohex-2-enyl)-vinyl]-benzene

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Chemical Name:1-Methoxy-2-((S)-2-methoxy-1-methyl-ethyl)-4-[(E)-2-((S)-2,6,6-trimethyl-cyclohex-2-enyl)-vinyl]-benzene
CAS No.:96641-57-5
Molecular Formula:C₂₂H₃₂O₂
Molecular Weight:328.495
Hs Code.:

Synonyms:1-Methoxy-2-((S)-2-methoxy-1-methyl-ethyl)-4-[(E)-2-((S)-2,6,6-trimethyl-cyclohex-2-enyl)-vinyl]-benzene

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Chemical Property of 1-Methoxy-2-((S)-2-methoxy-1-methyl-ethyl)-4-[(E)-2-((S)-2,6,6-trimethyl-cyclohex-2-enyl)-vinyl]-benzene

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Technology Process of 1-Methoxy-2-((S)-2-methoxy-1-methyl-ethyl)-4-[(E)-2-((S)-2,6,6-trimethyl-cyclohex-2-enyl)-vinyl]-benzene

There total 6 articles about 1-Methoxy-2-((S)-2-methoxy-1-methyl-ethyl)-4-[(E)-2-((S)-2,6,6-trimethyl-cyclohex-2-enyl)-vinyl]-benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 96641-44-0
(-)-(R)-2-(Orthomethoxy phenyl)propanol

: 96641-57-5
1-Methoxy-2-((S)-2-methoxy-1-methyl-ethyl)-4-[(E)-2-((S)-2,6,6-trimethyl-cyclohex-2-enyl)-vinyl]-benzene

Guidance literature:: Multi-step reaction with 4 steps

1: 95.5 percent / NaH / 1,2-dimethoxy-ethane / Ambient temperature

2: 5.90 g / AcOH / 6 h / 35 - 40 °C

3: 11.92 g / benzene / 1.5 h / Heating

4: 1)BuLi / 1)hexane,benzene, 10-20 deg C,5 min., 2) room temp. 1.5 h;

With n-butyllithium; sodium hydride; acetic acid; In 1,2-dimethoxyethane; benzene;
DOI:10.1246/bcsj.58.340

Reference yield:

: 81616-81-1
(R)-2-(2-methoxyphenyl)-propionic acid

: 96641-57-5
1-Methoxy-2-((S)-2-methoxy-1-methyl-ethyl)-4-[(E)-2-((S)-2,6,6-trimethyl-cyclohex-2-enyl)-vinyl]-benzene

Guidance literature:: Multi-step reaction with 6 steps

1: 91.6 percent / diethyl ether

2: 95.7 percent / LiAlH₄ / diethyl ether / 1.5 h / Ambient temperature

3: 95.5 percent / NaH / 1,2-dimethoxy-ethane / Ambient temperature

4: 5.90 g / AcOH / 6 h / 35 - 40 °C

5: 11.92 g / benzene / 1.5 h / Heating

6: 1)BuLi / 1)hexane,benzene, 10-20 deg C,5 min., 2) room temp. 1.5 h;

With lithium aluminium tetrahydride; n-butyllithium; sodium hydride; acetic acid; In 1,2-dimethoxyethane; diethyl ether; benzene;
DOI:10.1246/bcsj.58.340

Reference yield:

: 96687-72-8
Methyl (R)-(-)-2-(2-methoxyphenyl)propanoate

: 96641-57-5
1-Methoxy-2-((S)-2-methoxy-1-methyl-ethyl)-4-[(E)-2-((S)-2,6,6-trimethyl-cyclohex-2-enyl)-vinyl]-benzene

Guidance literature:: Multi-step reaction with 5 steps

1: 95.7 percent / LiAlH₄ / diethyl ether / 1.5 h / Ambient temperature

2: 95.5 percent / NaH / 1,2-dimethoxy-ethane / Ambient temperature

3: 5.90 g / AcOH / 6 h / 35 - 40 °C

4: 11.92 g / benzene / 1.5 h / Heating

5: 1)BuLi / 1)hexane,benzene, 10-20 deg C,5 min., 2) room temp. 1.5 h;

With lithium aluminium tetrahydride; n-butyllithium; sodium hydride; acetic acid; In 1,2-dimethoxyethane; diethyl ether; benzene;
DOI:10.1246/bcsj.58.340