[RhOs(CO)4((C₆H₅)2PCH₂P(C₆H₅)2)((C₆H₅)2PCH(CH₃)P(C₆H₅)2)]⁽¹⁺⁾*(CF₃SO₃)^(1-)=[RhOs(CO)4(C₆H₅)8P₄C₃H₆](CF₃SO₃)

Base Information

• Chemical Name: [RhOs(CO)4((C₆H₅)2PCH₂P(C₆H₅)2)((C₆H₅)2PCH(CH₃)P(C₆H₅)2)]⁽¹⁺⁾*(CF₃SO₃)^(1-)=[RhOs(CO)4(C₆H₅)8P₄C₃H₆](CF₃SO₃)
• CAS No.: 161205-32-9
• Molecular Formula: CF₃O₃S*C₅₅H₄₆O₄OsP₄Rh
• Molecular Weight: 1337.04

Synonyms:[RhOs(CO)4((C₆H₅)2PCH₂P(C₆H₅)2)((C₆H₅)2PCH(CH₃)P(C₆H₅)2)]⁽¹⁺⁾*(CF₃SO₃)^(1-)=[RhOs(CO)4(C₆H₅)8P₄C₃H₆](CF₃SO₃)

Chemical Property of [RhOs(CO)4((C₆H₅)2PCH₂P(C₆H₅)2)((C₆H₅)2PCH(CH₃)P(C₆H₅)2)]⁽¹⁺⁾*(CF₃SO₃)^(1-)=[RhOs(CO)4(C₆H₅)8P₄C₃H₆](CF₃SO₃)

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Technology Process of [RhOs(CO)4((C₆H₅)2PCH₂P(C₆H₅)2)((C₆H₅)2PCH(CH₃)P(C₆H₅)2)]⁽¹⁺⁾*(CF₃SO₃)^(1-)=[RhOs(CO)4(C₆H₅)8P₄C₃H₆](CF₃SO₃)

There total 2 articles about [RhOs(CO)4((C₆H₅)2PCH₂P(C₆H₅)2)((C₆H₅)2PCH(CH₃)P(C₆H₅)2)]⁽¹⁺⁾*(CF₃SO₃)^(1-)=[RhOs(CO)4(C₆H₅)8P₄C₃H₆](CF₃SO₃) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

RhOs(CO)4((C6H5)2PCHP(C6H5)2)((C6H5)2PCH2P(C6H5)2) + methyl trifluoromethanesulfonate (333-27-7) → [RhOs(CO)4((C6H5)2PCH2P(C6H5)2)((C6H5)2PCH(CH3)P(C6H5)2)](1+)*(CF3SO3)(1-)=[RhOs(CO)4(C6H5)8P4C3H6](CF3SO3) (161205-32-9)

Guidance literature:

In dichloromethane; stirring (1 h); crystn. (Et2O, 12 h), drying (vac.); elem. anal.;

DOI:10.1021/ja00106a028

Reference yield:

[RhOs(CO)4(dppm)2][BF4] (131178-41-1) → [RhOs(CO)4((C6H5)2PCH2P(C6H5)2)((C6H5)2PCH(CH3)P(C6H5)2)](1+)*(CF3SO3)(1-)=[RhOs(CO)4(C6H5)8P4C3H6](CF3SO3) (161205-32-9)

Guidance literature:

Multi-step reaction with 2 steps

1: C₄H₉Li / tetrahydrofuran; pentane

2: dichloromethane

With C₄H₉Li; In tetrahydrofuran; dichloromethane; pentane;

DOI:10.1021/ja00106a028

Reference yield: 85.0%

RhOs(CH3O2C3HCO2CH3)(CO)3((C6H5)2PCH2P(C6H5)2)2 + [RhOs(CO)4((C6H5)2PCH2P(C6H5)2)((C6H5)2PCH(CH3)P(C6H5)2)](1+)*(CF3SO3)(1-)=[RhOs(CO)4(C6H5)8P4C3H6](CF3SO3) (161205-32-9) → [RhOs((CH3)2(CO2)2C2H)(CH3)(CO)3((C6H5)2PCH2P(C6H5)2)2](1+)*[CF3SO3](1-)=[RhOs(C3O2H3)2H(CH3)(CO)3(C6H5)8P4(CH2)2]CF3SO3

Guidance literature:

In hexane; dichloromethane; stirring (1 h); recrystn. (CH2Cl2/hexanes), washing (hexanes), drying (vac.); elem. anal.;

DOI:10.1021/ja00106a028

upstream raw materials:

methyl trifluoromethanesulfonate

[RhOs(CO)4(dppm)2][BF₄]

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