3,5,6-trideoxy-3-(2-bromo-5-methoxybenzyl-para-toluenesulfonylamino)-1,2-O-isopropylidene-α-D-xylo-hexenofuranoside

Base Information

Chemical Name:3,5,6-trideoxy-3-(2-bromo-5-methoxybenzyl-para-toluenesulfonylamino)-1,2-O-isopropylidene-α-D-xylo-hexenofuranoside
CAS No.:869064-87-9
Molecular Formula:C₂₄H₂₈BrNO₆S
Molecular Weight:538.459
Hs Code.:

Synonyms:3,5,6-trideoxy-3-(2-bromo-5-methoxybenzyl-para-toluenesulfonylamino)-1,2-O-isopropylidene-α-D-xylo-hexenofuranoside

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Chemical Property of 3,5,6-trideoxy-3-(2-bromo-5-methoxybenzyl-para-toluenesulfonylamino)-1,2-O-isopropylidene-α-D-xylo-hexenofuranoside

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Technology Process of 3,5,6-trideoxy-3-(2-bromo-5-methoxybenzyl-para-toluenesulfonylamino)-1,2-O-isopropylidene-α-D-xylo-hexenofuranoside

There total 5 articles about 3,5,6-trideoxy-3-(2-bromo-5-methoxybenzyl-para-toluenesulfonylamino)-1,2-O-isopropylidene-α-D-xylo-hexenofuranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: N-(2-bromo-5-methoxy-benzyl)-N-[5-(1,2-dihydroxy-ethyl)-2,2-dimethyl-tetrahydro-furo[2,3-d][1,3]dioxol-6-yl]-4-methyl-benzenesulfonamide

: 869064-87-9
3,5,6-trideoxy-3-(2-bromo-5-methoxybenzyl-para-toluenesulfonylamino)-1,2-O-isopropylidene-α-D-xylo-hexenofuranoside

Guidance literature:: With 1H-imidazole; iodine; triphenylphosphine; In toluene; for 4h; Heating;
DOI:10.1055/s-2005-870012

Reference yield:

: 869064-85-7
3-deoxy-3-(2-bromo-5-methoxybenzyl-para-toluenesulfonylamino)-1,2:5,6-di-O-isopropylidene-α-D-glucofuranoside

: 869064-87-9
3,5,6-trideoxy-3-(2-bromo-5-methoxybenzyl-para-toluenesulfonylamino)-1,2-O-isopropylidene-α-D-xylo-hexenofuranoside

Guidance literature:: Multi-step reaction with 2 steps

1: aq. AcOH / 12 h / 20 °C

2: imidazole; Ph₃P; I₂ / toluene / 4 h / Heating

With 1H-imidazole; iodine; acetic acid; triphenylphosphine; In toluene;
DOI:10.1055/s-2005-870012

Reference yield:

: 98-59-9
p-toluenesulfonyl chloride

: 869064-87-9
3,5,6-trideoxy-3-(2-bromo-5-methoxybenzyl-para-toluenesulfonylamino)-1,2-O-isopropylidene-α-D-xylo-hexenofuranoside

Guidance literature:: Multi-step reaction with 4 steps

1: pyridine / 16 h / 20 °C

2: K₂CO₃ / acetone / 4 h / 20 °C

3: aq. AcOH / 12 h / 20 °C

4: imidazole; Ph₃P; I₂ / toluene / 4 h / Heating

With pyridine; 1H-imidazole; iodine; potassium carbonate; acetic acid; triphenylphosphine; In acetone; toluene;
DOI:10.1055/s-2005-870012