3-phenyl-6a,7-dihydro-3bH,6H-4-oxa-1,2,6,7a-tetraaza-cyclopenta[a]pentalen-5-one

Base Information

• Chemical Name: 3-phenyl-6a,7-dihydro-3bH,6H-4-oxa-1,2,6,7a-tetraaza-cyclopenta[a]pentalen-5-one
• CAS No.: 868762-38-3
• Molecular Formula: C₁₂H₁₀N₄O₂
• Molecular Weight: 242.237

Synonyms:3-phenyl-6a,7-dihydro-3bH,6H-4-oxa-1,2,6,7a-tetraaza-cyclopenta[a]pentalen-5-one

Chemical Property of 3-phenyl-6a,7-dihydro-3bH,6H-4-oxa-1,2,6,7a-tetraaza-cyclopenta[a]pentalen-5-one

Chemical Property:

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Technology Process of 3-phenyl-6a,7-dihydro-3bH,6H-4-oxa-1,2,6,7a-tetraaza-cyclopenta[a]pentalen-5-one

There total 4 articles about 3-phenyl-6a,7-dihydro-3bH,6H-4-oxa-1,2,6,7a-tetraaza-cyclopenta[a]pentalen-5-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

3-phenyl-6-(1-phenyl-ethyl)-6a,7-dihydro-3bH,6H-4-oxa-1,2,6,7a-tetraaza-cyclopenta[a]pentalen-5-one (868762-35-0) → 3-phenyl-6a,7-dihydro-3bH,6H-4-oxa-1,2,6,7a-tetraaza-cyclopenta[a]pentalen-5-one (868762-38-3)

Guidance literature:

With methanesulfonic acid; methoxybenzene; In chlorobenzene; Heating;

DOI:10.1055/s-2005-871974

Reference yield:

(R)-3-Phenyl-1-[(S)-1-((R)-1-phenyl-ethyl)-aziridin-2-yl]-prop-2-yn-1-ol → 3-phenyl-6a,7-dihydro-3bH,6H-4-oxa-1,2,6,7a-tetraaza-cyclopenta[a]pentalen-5-one (868762-38-3)

Guidance literature:

Multi-step reaction with 4 steps

1: azidotrimethylsilane / CH₂Cl₂ / 3 h / 20 °C

2: 106 mg / dimethylformamide / 16 h / 130 °C

3: 84 percent / NaH / tetrahydrofuran / -78 °C

4: 93 percent / MeSO₃H; anisole / chlorobenzene / Heating

With methanesulfonic acid; trimethylsilylazide; sodium hydride; methoxybenzene; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; chlorobenzene;

DOI:10.1055/s-2005-871974

Reference yield:

(3R,4S)-5-Azido-1-phenyl-4-((R)-1-phenyl-ethylamino)-pent-1-yn-3-ol → 3-phenyl-6a,7-dihydro-3bH,6H-4-oxa-1,2,6,7a-tetraaza-cyclopenta[a]pentalen-5-one (868762-38-3)

Guidance literature:

Multi-step reaction with 3 steps

1: 106 mg / dimethylformamide / 16 h / 130 °C

2: 84 percent / NaH / tetrahydrofuran / -78 °C

3: 93 percent / MeSO₃H; anisole / chlorobenzene / Heating

With methanesulfonic acid; sodium hydride; methoxybenzene; In tetrahydrofuran; N,N-dimethyl-formamide; chlorobenzene;

DOI:10.1055/s-2005-871974

upstream raw materials:

3-phenyl-6-(1-phenyl-ethyl)-6a,7-dihydro-3bH,6H-4-oxa-1,2,6,7a-tetraaza-cyclopenta[a]pentalen-5-one

(4S,5S)-4-hydroxy-3-phenyl-5-{(1R)-1-phenylethylamino}-5,6-dihydro-4H-pyrrolo[1,2-c][1,2,3]triazole

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