succinic acid mono-[5-(4-nitro-benzenesulfonyl)-1-(2-nitro-imidazol-1-ylmethyl)-pent-3-ynyl] ester

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Chemical Name:succinic acid mono-[5-(4-nitro-benzenesulfonyl)-1-(2-nitro-imidazol-1-ylmethyl)-pent-3-ynyl] ester
CAS No.:710337-22-7
Molecular Formula:C₁₉H₁₈N₄O₁₀S
Molecular Weight:494.439
Hs Code.:

Synonyms:succinic acid mono-[5-(4-nitro-benzenesulfonyl)-1-(2-nitro-imidazol-1-ylmethyl)-pent-3-ynyl] ester

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Chemical Property of succinic acid mono-[5-(4-nitro-benzenesulfonyl)-1-(2-nitro-imidazol-1-ylmethyl)-pent-3-ynyl] ester

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Technology Process of succinic acid mono-[5-(4-nitro-benzenesulfonyl)-1-(2-nitro-imidazol-1-ylmethyl)-pent-3-ynyl] ester

There total 4 articles about succinic acid mono-[5-(4-nitro-benzenesulfonyl)-1-(2-nitro-imidazol-1-ylmethyl)-pent-3-ynyl] ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 30.0%

: 710337-21-6
succinic acid mono-[1-(2-nitro-imidazol-1-ylmethyl)-5-(4-nitro-phenylsulfanyl)-pent-3-ynyl] ester

: 710337-22-7
succinic acid mono-[5-(4-nitro-benzenesulfonyl)-1-(2-nitro-imidazol-1-ylmethyl)-pent-3-ynyl] ester

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 0 ℃;
DOI:10.1016/j.bmcl.2004.02.060

Reference yield:

: 122951-69-3
1-Chloro-6-(tetrahydro-pyran-2-yloxy)-hex-4-yn-2-ol

: 710337-22-7
succinic acid mono-[5-(4-nitro-benzenesulfonyl)-1-(2-nitro-imidazol-1-ylmethyl)-pent-3-ynyl] ester

Guidance literature:: Multi-step reaction with 9 steps

1: 67 percent / aq. NaOH / ethanol / 20 °C

2: 72 percent / K₂CO₃ / ethanol / 70 °C

3: 88 percent / DMAP / CH₂Cl₂ / 20 °C

4: 94 percent / PPTS; MeOH / 20 °C

5: Et₃N / CH₂Cl₂ / 20 °C

6: NaH / CH₂Cl₂ / 20 °C

7: 88 percent / aq. NaOH / CH₂Cl₂; methanol / 20 °C

8: 94 percent / DMAP / CH₂Cl₂ / 20 °C

9: 30 percent / mCPBA / CH₂Cl₂ / 0 °C

With methanol; dmap; sodium hydroxide; pyridinium p-toluenesulfonate; sodium hydride; potassium carbonate; triethylamine; 3-chloro-benzenecarboperoxoic acid; In methanol; ethanol; dichloromethane;
DOI:10.1016/j.bmcl.2004.02.060

Reference yield:

: 710337-16-9
acetic acid 5-hydroxy-1-(2-nitro-imidazol-1-ylmethyl)-pent-3-ynyl ester

: 710337-22-7
succinic acid mono-[5-(4-nitro-benzenesulfonyl)-1-(2-nitro-imidazol-1-ylmethyl)-pent-3-ynyl] ester

Guidance literature:: Multi-step reaction with 5 steps

1: Et₃N / CH₂Cl₂ / 20 °C

2: NaH / CH₂Cl₂ / 20 °C

3: 88 percent / aq. NaOH / CH₂Cl₂; methanol / 20 °C

4: 94 percent / DMAP / CH₂Cl₂ / 20 °C

5: 30 percent / mCPBA / CH₂Cl₂ / 0 °C

With dmap; sodium hydroxide; sodium hydride; triethylamine; 3-chloro-benzenecarboperoxoic acid; In methanol; dichloromethane;
DOI:10.1016/j.bmcl.2004.02.060