3-(2-Oxo-1,2-dihydroquinoxalin-3-yl)-5,6,7,8-tetrafluoro-1-phenyl-1,4-dihydro-4-cinnolinone

Base Information

Chemical Name:3-(2-Oxo-1,2-dihydroquinoxalin-3-yl)-5,6,7,8-tetrafluoro-1-phenyl-1,4-dihydro-4-cinnolinone
CAS No.:220206-01-9
Molecular Formula:C₂₂H₁₀F₄N₄O₂
Molecular Weight:438.341
Hs Code.:

Synonyms:3-(2-Oxo-1,2-dihydroquinoxalin-3-yl)-5,6,7,8-tetrafluoro-1-phenyl-1,4-dihydro-4-cinnolinone

Suppliers and Price of 3-(2-Oxo-1,2-dihydroquinoxalin-3-yl)-5,6,7,8-tetrafluoro-1-phenyl-1,4-dihydro-4-cinnolinone

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 3-(2-Oxo-1,2-dihydroquinoxalin-3-yl)-5,6,7,8-tetrafluoro-1-phenyl-1,4-dihydro-4-cinnolinone

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 3-(2-Oxo-1,2-dihydroquinoxalin-3-yl)-5,6,7,8-tetrafluoro-1-phenyl-1,4-dihydro-4-cinnolinone

There total 8 articles about 3-(2-Oxo-1,2-dihydroquinoxalin-3-yl)-5,6,7,8-tetrafluoro-1-phenyl-1,4-dihydro-4-cinnolinone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 2-Oxo-3-(2-oxo-1-phenylhydrazo-2-pentafluorophenyl)ethylidene-1,2,3,4-tetrahydroquinoxaline

: 220206-01-9
3-(2-Oxo-1,2-dihydroquinoxalin-3-yl)-5,6,7,8-tetrafluoro-1-phenyl-1,4-dihydro-4-cinnolinone

Guidance literature:: at 280 - 290 ℃; for 0.0333333h;
DOI:10.1016/S0022-1139(98)00247-4

Reference yield:

: 100-34-5
benzene diazonium chloride

: 220206-01-9
3-(2-Oxo-1,2-dihydroquinoxalin-3-yl)-5,6,7,8-tetrafluoro-1-phenyl-1,4-dihydro-4-cinnolinone

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) HCl, NaNO₂ / 1.) H₂O, 0-5 deg C, 2.) H₂O, MeOH

2: 88 percent / diethyl ether / 1 h / Heating

3: 100 percent / 0.03 h / 280 - 290 °C

With hydrogenchloride; sodium nitrite; In diethyl ether;
DOI:10.1016/S0022-1139(98)00247-4

Reference yield:

: 62-53-3
aniline

: 220206-01-9
3-(2-Oxo-1,2-dihydroquinoxalin-3-yl)-5,6,7,8-tetrafluoro-1-phenyl-1,4-dihydro-4-cinnolinone

Guidance literature:: Multi-step reaction with 3 steps

1.1: HCl; H₂O; NaNO₂

1.2: 91 percent / NaOAc

2.1: 88 percent / diethyl ether / 1 h / Heating

3.1: 100 percent / 0.08 h / 280 - 290 °C

With hydrogenchloride; water; sodium nitrite; In diethyl ether; 1.1: Diazotization / 1.2: Addition / 2.1: Cyclization / 3.1: Cyclization;