C₂₉H₃₈B₂O₈

Base Information

Chemical Name:C₂₉H₃₈B₂O₈
CAS No.:1400055-44-8
Molecular Formula:C₂₉H₃₈B₂O₈
Molecular Weight:536.238
Hs Code.:

C<sub>29</sub>H<sub>38</sub>B<sub>2</sub>O<sub>8</sub>

Synonyms:C₂₉H₃₈B₂O₈

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Chemical Property of C₂₉H₃₈B₂O₈

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Technology Process of C₂₉H₃₈B₂O₈

There total 5 articles about C₂₉H₃₈B₂O₈ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

: 1400055-39-1
C₁₇H₁₄Br₂O₄

: 25015-63-8
4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane

: 1400055-44-8
C₂₉H₃₈B₂O₈

Guidance literature:: With [1,3-bis(2,6-diisopropylphenyl)imidazol-2-ylidene](3-chloropyridyl) palladium(II) dichloride; triethylamine; at 110 ℃;
DOI:10.1021/ol302273r DOI:10.1021/ol302273r

Reference yield:

: 74003-55-7
3,4-dibromobenzaldehyde

: 1400055-44-8
C₂₉H₃₈B₂O₈

Guidance literature:: Multi-step reaction with 4 steps

1.1: piperdinium acetate / benzene / 6 h / Reflux

2.1: 9-O-benzylcupreidine / toluene / 48 h / 23 °C / Reflux

2.2: 2 h / 80 °C

3.1: bis-[(trifluoroacetoxy)iodo]benzene; formic acid; sulfuric acid / 12 h / 23 °C / Cooling with ice; Inert atmosphere

4.1: [1,3-bis(2,6-diisopropylphenyl)imidazol-2-ylidene](3-chloropyridyl) palladium(II) dichloride; triethylamine / 110 °C

With 9-O-benzylcupreidine; formic acid; [1,3-bis(2,6-diisopropylphenyl)imidazol-2-ylidene](3-chloropyridyl) palladium(II) dichloride; sulfuric acid; piperdinium acetate; triethylamine; bis-[(trifluoroacetoxy)iodo]benzene; In toluene; benzene; 1.1: |Knoevenagel Condensation;
DOI:10.1021/ol302273r DOI:10.1021/ol302273r

Reference yield:

: 1351365-53-1
C₁₄H₁₈O₅

: 1400055-44-8
C₂₉H₃₈B₂O₈

Guidance literature:: Multi-step reaction with 4 steps

1.1: piperdinium acetate / benzene / 6 h / Reflux

2.1: 9-O-benzylcupreidine / toluene / 48 h / 23 °C / Reflux

2.2: 2 h / 80 °C

3.1: bis-[(trifluoroacetoxy)iodo]benzene; formic acid; sulfuric acid / 12 h / 23 °C / Cooling with ice; Inert atmosphere

4.1: [1,3-bis(2,6-diisopropylphenyl)imidazol-2-ylidene](3-chloropyridyl) palladium(II) dichloride; triethylamine / 110 °C

With 9-O-benzylcupreidine; formic acid; [1,3-bis(2,6-diisopropylphenyl)imidazol-2-ylidene](3-chloropyridyl) palladium(II) dichloride; sulfuric acid; piperdinium acetate; triethylamine; bis-[(trifluoroacetoxy)iodo]benzene; In toluene; benzene; 1.1: |Knoevenagel Condensation;
DOI:10.1021/ol302273r DOI:10.1021/ol302273r