Technology Process of C36H62O5Si2
There total 6 articles about C36H62O5Si2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
potassium carbonate;
In
acetone;
at 20 ℃;
for 18h;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: 1H-imidazole / dichloromethane / 18 h / 20 °C
2.1: diisobutylaluminium hydride / dichloromethane; hexane / 0.5 h / -30 °C / Inert atmosphere
2.2: -30 °C
3.1: potassium tert-butylate / tetrahydrofuran / 0.5 h / 20 °C / Inert atmosphere
3.2: 3.25 h / 0 - 20 °C
4.1: potassium carbonate / acetone / 18 h / 20 °C
With
1H-imidazole; potassium tert-butylate; diisobutylaluminium hydride; potassium carbonate;
In
tetrahydrofuran; hexane; dichloromethane; acetone;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: (-)-diisopinocamphenylborane chloride / n-heptane; tetrahydrofuran / 5 h / -30 - -25 °C / Inert atmosphere
1.2: 10 h / 20 °C
2.1: 1H-imidazole / dichloromethane / 18 h / 20 °C
3.1: diisobutylaluminium hydride / dichloromethane; hexane / 0.5 h / -30 °C / Inert atmosphere
3.2: -30 °C
4.1: potassium tert-butylate / tetrahydrofuran / 0.5 h / 20 °C / Inert atmosphere
4.2: 3.25 h / 0 - 20 °C
5.1: potassium carbonate / acetone / 18 h / 20 °C
With
1H-imidazole; potassium tert-butylate; diisobutylaluminium hydride; potassium carbonate; (-)-diisopinocamphenylborane chloride;
In
tetrahydrofuran; hexane; n-heptane; dichloromethane; acetone;