Technology Process of N,N-diallyl-α-(phenylthio)acetamide
There total 1 articles about N,N-diallyl-α-(phenylthio)acetamide which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
2-chloro-1-methyl-pyridinium iodide; triethylamine;
In
dichloromethane;
Ambient temperature;
DOI:10.1246/bcsj.66.1496
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 1.) potassium t-butoxide, LDA, 2.) p-MeC6H4SO2N3 / 1.) THF, 0.5 h, 2.) THF, RT, 8 h
2: 60 percent / LiAlH4, CuCl2 / tetrahydrofuran / 0.5 h / Ambient temperature
3: potassium t-butoxide / dimethylsulfoxide / 0.17 h / Ambient temperature
4: NaOH, 4percent aq. KMnO4 / methanol
With
sodium hydroxide; potassium permanganate; lithium aluminium tetrahydride; 4-toluenesulfonyl azide; potassium tert-butylate; copper dichloride; lithium diisopropyl amide;
In
tetrahydrofuran; methanol; dimethyl sulfoxide;
DOI:10.1246/bcsj.66.1496
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 1.) potassium t-butoxide, LDA, 2.) p-MeC6H4SO2N3 / 1.) THF, 0.5 h, 2.) THF, RT, 8 h
2: 60 percent / LiAlH4, CuCl2 / tetrahydrofuran / 0.5 h / Ambient temperature
3: potassium t-butoxide / dimethylsulfoxide / 0.17 h / Ambient temperature
With
lithium aluminium tetrahydride; 4-toluenesulfonyl azide; potassium tert-butylate; copper dichloride; lithium diisopropyl amide;
In
tetrahydrofuran; dimethyl sulfoxide;
DOI:10.1246/bcsj.66.1496
