(+)-(1S,2S)-(2-allyl-1,3,3-trimethylcyclohexyl)methanol

Base Information

Chemical Name:(+)-(1S,2S)-(2-allyl-1,3,3-trimethylcyclohexyl)methanol
CAS No.:97855-70-4
Molecular Formula:C₁₃H₂₄O
Molecular Weight:196.333
Hs Code.:

Synonyms:(+)-(1S,2S)-(2-allyl-1,3,3-trimethylcyclohexyl)methanol

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Chemical Property of (+)-(1S,2S)-(2-allyl-1,3,3-trimethylcyclohexyl)methanol

Chemical Property:

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Technology Process of (+)-(1S,2S)-(2-allyl-1,3,3-trimethylcyclohexyl)methanol

There total 10 articles about (+)-(1S,2S)-(2-allyl-1,3,3-trimethylcyclohexyl)methanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 110715-80-5
(-)-(1S,8aS)-1,2,3,5,6,7,8,8a-octahydro-5,5,8a-trimethylnaphthalen-1-ol

: 97855-70-4
(+)-(1S,2S)-(2-allyl-1,3,3-trimethylcyclohexyl)methanol

Guidance literature:: Multi-step reaction with 9 steps

1: 95 percent / H₂ / Adam's catalyst / acetic acid

2: 90 percent / Florisil, PCC / CH₂Cl₂ / 2 h / Ambient temperature

3: 97 percent / PBB / acetic acid / 2 h / Ambient temperature

4: 97 percent / sodium hydroxide / dimethylformamide; H₂O / 0.5 h / Ambient temperature

5: lead tetra-acetate (LTA) / benzene / 0.17 h / Ambient temperature

6: NaBH₄ / methanol / 0.33 h / Ambient temperature

7: 98 percent / tributylphosphine / tetrahydrofuran / 0.33 h / Ambient temperature

8: 91 percent / hydrogen peroxide / tetrahydrofuran / 10 h / Ambient temperature

9: 1.) lithium aluminium hydride; 2.) sodium hydroxide / 1.) diethyl ether, rt, 30 min; 2.) water, 30 min.

With lead(IV) acetate; sodium hydroxide; sodium tetrahydroborate; florisil; lithium aluminium tetrahydride; tributylphosphine; hydrogen; dihydrogen peroxide; pyridinium chlorochromate; platinum(IV) oxide; In tetrahydrofuran; methanol; dichloromethane; water; acetic acid; N,N-dimethyl-formamide; benzene;

Reference yield:

: 110654-75-6
(+)-(4aS,5S)-5-benzoyloxy-3,4,4a,5,6,7-hexahydro-1,1,4a-trimethylnaphthalen-2(1H)-one

: 97855-70-4
(+)-(1S,2S)-(2-allyl-1,3,3-trimethylcyclohexyl)methanol

Guidance literature:: Multi-step reaction with 10 steps

1: 93 percent / potassium hydroxide, hydrazine hydrate / bis-(2-hydroxy-ethyl) ether / 6 h / Heating

2: 95 percent / H₂ / Adam's catalyst / acetic acid

3: 90 percent / Florisil, PCC / CH₂Cl₂ / 2 h / Ambient temperature

4: 97 percent / PBB / acetic acid / 2 h / Ambient temperature

5: 97 percent / sodium hydroxide / dimethylformamide; H₂O / 0.5 h / Ambient temperature

6: lead tetra-acetate (LTA) / benzene / 0.17 h / Ambient temperature

7: NaBH₄ / methanol / 0.33 h / Ambient temperature

8: 98 percent / tributylphosphine / tetrahydrofuran / 0.33 h / Ambient temperature

9: 91 percent / hydrogen peroxide / tetrahydrofuran / 10 h / Ambient temperature

10: 1.) lithium aluminium hydride; 2.) sodium hydroxide / 1.) diethyl ether, rt, 30 min; 2.) water, 30 min.

With lead(IV) acetate; potassium hydroxide; sodium hydroxide; sodium tetrahydroborate; florisil; lithium aluminium tetrahydride; tributylphosphine; hydrogen; dihydrogen peroxide; hydrazine hydrate; pyridinium chlorochromate; platinum(IV) oxide; In tetrahydrofuran; methanol; dichloromethane; water; acetic acid; N,N-dimethyl-formamide; diethylene glycol; benzene;

Reference yield:

: 97855-69-1
methyl (+)-(1S,2S)-2-allyl-1,3,3-trimethylcyclohexanecarboxylate

: 97855-70-4
(+)-(1S,2S)-(2-allyl-1,3,3-trimethylcyclohexyl)methanol

Guidance literature:: With sodium hydroxide; lithium aluminium tetrahydride; Yield given. Multistep reaction; 1.) diethyl ether, rt, 30 min; 2.) water, 30 min.;