(1S,2S)-2-Allyl-1,3,3-trimethyl-cyclohexanecarbaldehyde

Base Information

Chemical Name:(1S,2S)-2-Allyl-1,3,3-trimethyl-cyclohexanecarbaldehyde
CAS No.:110654-68-7
Molecular Formula:C₁₃H₂₂O
Molecular Weight:194.317
Hs Code.:

Synonyms:(1S,2S)-2-Allyl-1,3,3-trimethyl-cyclohexanecarbaldehyde

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Chemical Property of (1S,2S)-2-Allyl-1,3,3-trimethyl-cyclohexanecarbaldehyde

Chemical Property:

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Technology Process of (1S,2S)-2-Allyl-1,3,3-trimethyl-cyclohexanecarbaldehyde

There total 11 articles about (1S,2S)-2-Allyl-1,3,3-trimethyl-cyclohexanecarbaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 97855-70-4
(+)-(1S,2S)-(2-allyl-1,3,3-trimethylcyclohexyl)methanol

: 110654-68-7
(1S,2S)-2-Allyl-1,3,3-trimethyl-cyclohexanecarbaldehyde

Guidance literature:: With florisil; pyridinium chlorochromate; In dichloromethane; for 1h; Ambient temperature;

Reference yield:

: 110715-80-5
(-)-(1S,8aS)-1,2,3,5,6,7,8,8a-octahydro-5,5,8a-trimethylnaphthalen-1-ol

: 110654-68-7
(1S,2S)-2-Allyl-1,3,3-trimethyl-cyclohexanecarbaldehyde

Guidance literature:: Multi-step reaction with 10 steps

1: 95 percent / H₂ / Adam's catalyst / acetic acid

2: 90 percent / Florisil, PCC / CH₂Cl₂ / 2 h / Ambient temperature

3: 97 percent / PBB / acetic acid / 2 h / Ambient temperature

4: 97 percent / sodium hydroxide / dimethylformamide; H₂O / 0.5 h / Ambient temperature

5: lead tetra-acetate (LTA) / benzene / 0.17 h / Ambient temperature

6: NaBH₄ / methanol / 0.33 h / Ambient temperature

7: 98 percent / tributylphosphine / tetrahydrofuran / 0.33 h / Ambient temperature

8: 91 percent / hydrogen peroxide / tetrahydrofuran / 10 h / Ambient temperature

9: 1.) lithium aluminium hydride; 2.) sodium hydroxide / 1.) diethyl ether, rt, 30 min; 2.) water, 30 min.

10: 88 percent / Florisil, PCC / CH₂Cl₂ / 1 h / Ambient temperature

With lead(IV) acetate; sodium hydroxide; sodium tetrahydroborate; florisil; lithium aluminium tetrahydride; tributylphosphine; hydrogen; dihydrogen peroxide; pyridinium chlorochromate; platinum(IV) oxide; In tetrahydrofuran; methanol; dichloromethane; water; acetic acid; N,N-dimethyl-formamide; benzene;

Reference yield:

: 110654-75-6
(+)-(4aS,5S)-5-benzoyloxy-3,4,4a,5,6,7-hexahydro-1,1,4a-trimethylnaphthalen-2(1H)-one

: 110654-68-7
(1S,2S)-2-Allyl-1,3,3-trimethyl-cyclohexanecarbaldehyde

Guidance literature:: Multi-step reaction with 11 steps

1: 93 percent / potassium hydroxide, hydrazine hydrate / bis-(2-hydroxy-ethyl) ether / 6 h / Heating

2: 95 percent / H₂ / Adam's catalyst / acetic acid

3: 90 percent / Florisil, PCC / CH₂Cl₂ / 2 h / Ambient temperature

4: 97 percent / PBB / acetic acid / 2 h / Ambient temperature

5: 97 percent / sodium hydroxide / dimethylformamide; H₂O / 0.5 h / Ambient temperature

6: lead tetra-acetate (LTA) / benzene / 0.17 h / Ambient temperature

7: NaBH₄ / methanol / 0.33 h / Ambient temperature

8: 98 percent / tributylphosphine / tetrahydrofuran / 0.33 h / Ambient temperature

9: 91 percent / hydrogen peroxide / tetrahydrofuran / 10 h / Ambient temperature

10: 1.) lithium aluminium hydride; 2.) sodium hydroxide / 1.) diethyl ether, rt, 30 min; 2.) water, 30 min.

11: 88 percent / Florisil, PCC / CH₂Cl₂ / 1 h / Ambient temperature

With lead(IV) acetate; potassium hydroxide; sodium hydroxide; sodium tetrahydroborate; florisil; lithium aluminium tetrahydride; tributylphosphine; hydrogen; dihydrogen peroxide; hydrazine hydrate; pyridinium chlorochromate; platinum(IV) oxide; In tetrahydrofuran; methanol; dichloromethane; water; acetic acid; N,N-dimethyl-formamide; diethylene glycol; benzene;