N-(benzyloxycarbonyl)aminopropyl 2-acetamido-3,4,6-tri-O-benzyl-2-deoxy-β-D-mannopyranoside

Base Information

Chemical Name:N-(benzyloxycarbonyl)aminopropyl 2-acetamido-3,4,6-tri-O-benzyl-2-deoxy-β-D-mannopyranoside
CAS No.:858109-00-9
Molecular Formula:C₄₀H₄₆N₂O₈
Molecular Weight:682.814
Hs Code.:

Synonyms:N-(benzyloxycarbonyl)aminopropyl 2-acetamido-3,4,6-tri-O-benzyl-2-deoxy-β-D-mannopyranoside

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Chemical Property of N-(benzyloxycarbonyl)aminopropyl 2-acetamido-3,4,6-tri-O-benzyl-2-deoxy-β-D-mannopyranoside

Chemical Property:

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Technology Process of N-(benzyloxycarbonyl)aminopropyl 2-acetamido-3,4,6-tri-O-benzyl-2-deoxy-β-D-mannopyranoside

There total 7 articles about N-(benzyloxycarbonyl)aminopropyl 2-acetamido-3,4,6-tri-O-benzyl-2-deoxy-β-D-mannopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: [3-((2R,3S,4R,5S,6R)-3-Amino-4,5-bis-benzyloxy-6-benzyloxymethyl-tetrahydro-pyran-2-yloxy)-propyl]-carbamic acid benzyl ester

: 108-24-7
acetic anhydride

: 858109-00-9
N-(benzyloxycarbonyl)aminopropyl 2-acetamido-3,4,6-tri-O-benzyl-2-deoxy-β-D-mannopyranoside

Guidance literature:: In methanol; at 20 ℃;
DOI:10.1055/s-2005-865226

Reference yield:

: 858108-96-0
N-(benzyloxycarbonyl)aminopropyl 3,4,6-tri-O-benzyl-β-D-glucopyranoside

: 858109-00-9
N-(benzyloxycarbonyl)aminopropyl 2-acetamido-3,4,6-tri-O-benzyl-2-deoxy-β-D-mannopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1: pyridine / CH₂Cl₂ / 0 °C

2: tetrabutylammonium azide / toluene / 60 °C

3: Et₃N; HS(CH₂)3SH / methanol / 90 °C

4: methanol / 20 °C

With pyridine; 1.3-propanedithiol; tetrabutylammoniun azide; triethylamine; In methanol; dichloromethane; toluene;
DOI:10.1055/s-2005-865226

Reference yield:

: 858108-98-2
N-(benzyloxycarbonyl)aminopropyl 2-azido-3,4,6-tri-O-benzyl-2-deoxy-β-D-mannopyranoside

: 858109-00-9
N-(benzyloxycarbonyl)aminopropyl 2-acetamido-3,4,6-tri-O-benzyl-2-deoxy-β-D-mannopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: Et₃N; HS(CH₂)3SH / methanol / 90 °C

2: methanol / 20 °C

With 1.3-propanedithiol; triethylamine; In methanol;
DOI:10.1055/s-2005-865226