{(2R,4aR,6S,7R,8R,8aS)-6-[tert-Butyl-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluoro-decyloxy)-phenyl-silanyloxy]-8-hydroxy-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-7-yl}-carbamic acid 2,2,2-trichloro-ethyl ester

Base Information

Chemical Name:{(2R,4aR,6S,7R,8R,8aS)-6-[tert-Butyl-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluoro-decyloxy)-phenyl-silanyloxy]-8-hydroxy-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-7-yl}-carbamic acid 2,2,2-trichloro-ethyl ester
CAS No.:807355-18-6
Molecular Formula:C₃₆H₃₅Cl₃F₁₇NO₈Si
Molecular Weight:1067.09
Hs Code.:

{(2R,4aR,6S,7R,8R,8aS)-6-[tert-Butyl-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluoro-decyloxy)-phenyl-silanyloxy]-8-hydroxy-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-7-yl}-carbamic acid 2,2,2-trichloro-ethyl ester

Synonyms:{(2R,4aR,6S,7R,8R,8aS)-6-[tert-Butyl-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluoro-decyloxy)-phenyl-silanyloxy]-8-hydroxy-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-7-yl}-carbamic acid 2,2,2-trichloro-ethyl ester

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Chemical Property of {(2R,4aR,6S,7R,8R,8aS)-6-[tert-Butyl-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluoro-decyloxy)-phenyl-silanyloxy]-8-hydroxy-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-7-yl}-carbamic acid 2,2,2-trichloro-ethyl ester

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Technology Process of {(2R,4aR,6S,7R,8R,8aS)-6-[tert-Butyl-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluoro-decyloxy)-phenyl-silanyloxy]-8-hydroxy-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-7-yl}-carbamic acid 2,2,2-trichloro-ethyl ester

There total 3 articles about {(2R,4aR,6S,7R,8R,8aS)-6-[tert-Butyl-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluoro-decyloxy)-phenyl-silanyloxy]-8-hydroxy-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-7-yl}-carbamic acid 2,2,2-trichloro-ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 136945-13-6,136945-23-8
[(2R,3S,4R,5R)-3,4-diacetoxy-6-hydroxy-5-(2,2,2-trichloroethoxycarbonylamino)tetrahydropyran-2-yl]methyl acetate

: 807355-18-6
{(2R,4aR,6S,7R,8R,8aS)-6-[tert-Butyl-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluoro-decyloxy)-phenyl-silanyloxy]-8-hydroxy-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-7-yl}-carbamic acid 2,2,2-trichloro-ethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 98 percent / Et₃N; dimethylaminopyridine / CH₂Cl₂ / 20 °C

2: NaOMe / methanol / 2 h / 20 °C

3: 0.885 g / camphorsulfonic acid / acetonitrile / 3 h / 20 °C

With dmap; camphor-10-sulfonic acid; sodium methylate; triethylamine; In methanol; dichloromethane; acetonitrile;
DOI:10.1021/ol048474g

Reference yield:

: 243645-01-4
tert-butyl-phenyl-1H,1H,2H,2H-heptadecafluorodecyloxysilyl bromide

: 807355-18-6
{(2R,4aR,6S,7R,8R,8aS)-6-[tert-Butyl-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluoro-decyloxy)-phenyl-silanyloxy]-8-hydroxy-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-7-yl}-carbamic acid 2,2,2-trichloro-ethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 98 percent / Et₃N; dimethylaminopyridine / CH₂Cl₂ / 20 °C

2: NaOMe / methanol / 2 h / 20 °C

3: 0.885 g / camphorsulfonic acid / acetonitrile / 3 h / 20 °C

With dmap; camphor-10-sulfonic acid; sodium methylate; triethylamine; In methanol; dichloromethane; acetonitrile;
DOI:10.1021/ol048474g

Reference yield:

: 807355-16-4
Acetic acid (2R,3S,4R,5R,6S)-3-acetoxy-2-acetoxymethyl-6-[tert-butyl-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluoro-decyloxy)-phenyl-silanyloxy]-5-(2,2,2-trichloro-ethoxycarbonylamino)-tetrahydro-pyran-4-yl ester

: 807355-18-6
{(2R,4aR,6S,7R,8R,8aS)-6-[tert-Butyl-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluoro-decyloxy)-phenyl-silanyloxy]-8-hydroxy-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-7-yl}-carbamic acid 2,2,2-trichloro-ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: NaOMe / methanol / 2 h / 20 °C

2: 0.885 g / camphorsulfonic acid / acetonitrile / 3 h / 20 °C

With camphor-10-sulfonic acid; sodium methylate; In methanol; acetonitrile;
DOI:10.1021/ol048474g