benzyl 6-O-acetyl-3-deoxy-4-S-benzyl-4-thio-α-D-threo-hexopyranosid-2-ulose

Base Information

Chemical Name:benzyl 6-O-acetyl-3-deoxy-4-S-benzyl-4-thio-α-D-threo-hexopyranosid-2-ulose
CAS No.:463935-93-5
Molecular Formula:C₂₂H₂₄O₅S
Molecular Weight:400.496
Hs Code.:

Synonyms:benzyl 6-O-acetyl-3-deoxy-4-S-benzyl-4-thio-α-D-threo-hexopyranosid-2-ulose

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of benzyl 6-O-acetyl-3-deoxy-4-S-benzyl-4-thio-α-D-threo-hexopyranosid-2-ulose

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Technology Process of benzyl 6-O-acetyl-3-deoxy-4-S-benzyl-4-thio-α-D-threo-hexopyranosid-2-ulose

There total 3 articles about benzyl 6-O-acetyl-3-deoxy-4-S-benzyl-4-thio-α-D-threo-hexopyranosid-2-ulose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 100-53-8
phenylmethanethiol

: 463935-90-2
benzyl 6-O-acetyl-3,4-dideoxy-α-D-glycero-hex-3-enopyranosid-2-ulose

: 463935-93-5
benzyl 6-O-acetyl-3-deoxy-4-S-benzyl-4-thio-α-D-threo-hexopyranosid-2-ulose

Guidance literature:: With triethylamine; In dichloromethane; at 50 ℃; for 5h;
DOI:10.1071/CH01200

Reference yield:

: 100-51-6,185532-71-2
benzyl alcohol

: 463935-93-5
benzyl 6-O-acetyl-3-deoxy-4-S-benzyl-4-thio-α-D-threo-hexopyranosid-2-ulose

Guidance literature:: Multi-step reaction with 2 steps

1: 76 percent / SnCl₄ / CH₂Cl₂ / 3 h / -20 °C

2: 88 percent / Et₃N / CH₂Cl₂ / 5 h / 50 °C

With tin(IV) chloride; triethylamine; In dichloromethane; 2: Michael addition;
DOI:10.1071/CH01200

Reference yield:

: 14125-78-1
2,3,4,6-tetra-O-acetyl-1,5-anhydro-D-lyxo-hex-1-enitol

: 463935-93-5
benzyl 6-O-acetyl-3-deoxy-4-S-benzyl-4-thio-α-D-threo-hexopyranosid-2-ulose

Guidance literature:: Multi-step reaction with 2 steps

1: 76 percent / SnCl₄ / CH₂Cl₂ / 3 h / -20 °C

2: 88 percent / Et₃N / CH₂Cl₂ / 5 h / 50 °C

With tin(IV) chloride; triethylamine; In dichloromethane; 2: Michael addition;
DOI:10.1071/CH01200