N-succinimidyl 5-((3-((4'-chloro-[1,1'-biphenyl]-2-yl)carbamoyl)pyridin-2-yl)thio)pentanoate

Base Information

Chemical Name:N-succinimidyl 5-((3-((4'-chloro-[1,1'-biphenyl]-2-yl)carbamoyl)pyridin-2-yl)thio)pentanoate
CAS No.:1387582-17-3
Molecular Formula:C₂₇H₂₄ClN₃O₅S
Molecular Weight:538.024
Hs Code.:

Synonyms:N-succinimidyl 5-((3-((4'-chloro-[1,1'-biphenyl]-2-yl)carbamoyl)pyridin-2-yl)thio)pentanoate

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Chemical Property of N-succinimidyl 5-((3-((4'-chloro-[1,1'-biphenyl]-2-yl)carbamoyl)pyridin-2-yl)thio)pentanoate

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Technology Process of N-succinimidyl 5-((3-((4'-chloro-[1,1'-biphenyl]-2-yl)carbamoyl)pyridin-2-yl)thio)pentanoate

There total 6 articles about N-succinimidyl 5-((3-((4'-chloro-[1,1'-biphenyl]-2-yl)carbamoyl)pyridin-2-yl)thio)pentanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 74124-79-1
di(succinimido) carbonate

: 1375459-47-4
5-((3-((4'-chloro-[1,1'-biphenyl]-2-yl)carbamoyl)pyridin-2-yl)thio)pentanoic acid

: 1387582-17-3
N-succinimidyl 5-((3-((4'-chloro-[1,1'-biphenyl]-2-yl)carbamoyl)pyridin-2-yl)thio)pentanoate

Guidance literature:: With triethylamine; In acetonitrile; at 20 ℃; for 5h; Inert atmosphere;
DOI:10.1016/j.foodchem.2012.04.090

Reference yield:

: 1375459-46-3
methyl 5-((3-((4'-chloro-[1,1'-biphenyl]-2-yl)carbamoyl)pyridin-2-yl)thio)pentanoate

: 1387582-17-3
N-succinimidyl 5-((3-((4'-chloro-[1,1'-biphenyl]-2-yl)carbamoyl)pyridin-2-yl)thio)pentanoate

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydroxide / methanol; water / 4 h / 20 °C

2: triethylamine / acetonitrile / 5 h / 20 °C / Inert atmosphere

With triethylamine; sodium hydroxide; In methanol; water; acetonitrile;
DOI:10.1016/j.foodchem.2012.04.090

Reference yield:

: 1375459-44-1
2-(4-carboxybutylthio)nicotinic acid

: 1387582-17-3
N-succinimidyl 5-((3-((4'-chloro-[1,1'-biphenyl]-2-yl)carbamoyl)pyridin-2-yl)thio)pentanoate

Guidance literature:: Multi-step reaction with 5 steps

1: methanol; chloro-trimethyl-silane / 168 h / 20 °C

2: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 24 h / 20 °C

3: pyridine; dmap / dichloromethane / 72 h / 20 °C

4: sodium hydroxide / methanol; water / 4 h / 20 °C

5: triethylamine / acetonitrile / 5 h / 20 °C / Inert atmosphere

With pyridine; methanol; dmap; chloro-trimethyl-silane; oxalyl dichloride; triethylamine; N,N-dimethyl-formamide; sodium hydroxide; In methanol; dichloromethane; water; acetonitrile;
DOI:10.1016/j.foodchem.2012.04.090