3-(4-methoxyphenyl)-2-(4-nitrophenyl)-3,4-dihydro-2H-benzo[e][1,3]oxazine

Base Information

Chemical Name:3-(4-methoxyphenyl)-2-(4-nitrophenyl)-3,4-dihydro-2H-benzo[e][1,3]oxazine
CAS No.:1207178-64-0
Molecular Formula:C₂₁H₁₈N₂O₄
Molecular Weight:362.385
Hs Code.:

Synonyms:3-(4-methoxyphenyl)-2-(4-nitrophenyl)-3,4-dihydro-2H-benzo[e][1,3]oxazine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-(4-methoxyphenyl)-2-(4-nitrophenyl)-3,4-dihydro-2H-benzo[e][1,3]oxazine

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Technology Process of 3-(4-methoxyphenyl)-2-(4-nitrophenyl)-3,4-dihydro-2H-benzo[e][1,3]oxazine

There total 4 articles about 3-(4-methoxyphenyl)-2-(4-nitrophenyl)-3,4-dihydro-2H-benzo[e][1,3]oxazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 52537-88-9
N-(2-hydroxybenzyl)-p-anisidine

: 555-16-8
4-nitrobenzaldehdye

: 1207178-64-0
3-(4-methoxyphenyl)-2-(4-nitrophenyl)-3,4-dihydro-2H-benzo[e][1,3]oxazine

Guidance literature:: With tin(IV) chloride; In chloroform; cyclohexane; at 85 ℃; for 5h; Inert atmosphere; Dean-Stark trap;
DOI:10.1080/00397911.2010.540691

Reference yield:

: 90-02-8
salicylaldehyde

: 1207178-64-0
3-(4-methoxyphenyl)-2-(4-nitrophenyl)-3,4-dihydro-2H-benzo[e][1,3]oxazine

Guidance literature:: Multi-step reaction with 3 steps

1: ethanol / Reflux

2: sodium tetrahydroborate / methanol

3: tin(IV) chloride / chloroform; cyclohexane / 5 h / 85 °C / Inert atmosphere; Dean-Stark trap

With sodium tetrahydroborate; tin(IV) chloride; In methanol; ethanol; chloroform; cyclohexane; 1: Mannich reaction;
DOI:10.1080/00397911.2010.540691

Reference yield:

: 889-08-7,116546-10-2,117909-25-8
salicylidene-4-anisidine

: 1207178-64-0
3-(4-methoxyphenyl)-2-(4-nitrophenyl)-3,4-dihydro-2H-benzo[e][1,3]oxazine

Guidance literature:: Multi-step reaction with 2 steps

1: sodium tetrahydroborate / methanol

2: tin(IV) chloride / chloroform; cyclohexane / 5 h / 85 °C / Inert atmosphere; Dean-Stark trap

With sodium tetrahydroborate; tin(IV) chloride; In methanol; chloroform; cyclohexane;
DOI:10.1080/00397911.2010.540691