2-[3-(bromomethyl)-2,4,6-trimethylbenzyl]-4,4-dimethyl-4,5-dihydrooxazole

Base Information

Chemical Name:2-[3-(bromomethyl)-2,4,6-trimethylbenzyl]-4,4-dimethyl-4,5-dihydrooxazole
CAS No.:943757-07-1
Molecular Formula:C₁₆H₂₂BrNO
Molecular Weight:324.261
Hs Code.:

Synonyms:2-[3-(bromomethyl)-2,4,6-trimethylbenzyl]-4,4-dimethyl-4,5-dihydrooxazole

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Chemical Property of 2-[3-(bromomethyl)-2,4,6-trimethylbenzyl]-4,4-dimethyl-4,5-dihydrooxazole

Chemical Property:

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Technology Process of 2-[3-(bromomethyl)-2,4,6-trimethylbenzyl]-4,4-dimethyl-4,5-dihydrooxazole

There total 4 articles about 2-[3-(bromomethyl)-2,4,6-trimethylbenzyl]-4,4-dimethyl-4,5-dihydrooxazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 943757-06-0
{3-[(4,4-dimethyl-4,5-dihydrooxazol-2-yl)methyl]-2,4,6-trimethylphenyl}methanol

: 943757-07-1
2-[3-(bromomethyl)-2,4,6-trimethylbenzyl]-4,4-dimethyl-4,5-dihydrooxazole

Guidance literature:: With phosphorus tribromide; In tetrahydrofuran; at -20 ℃; for 1h;
DOI:10.1055/s-2007-965938

Reference yield:

: 943757-04-8
[3-(hydroxymethyl)-2,4,6-trimethylphenyl]acetonitrile

: 943757-07-1
2-[3-(bromomethyl)-2,4,6-trimethylbenzyl]-4,4-dimethyl-4,5-dihydrooxazole

Guidance literature:: Multi-step reaction with 2 steps

1: 52 percent / Cd(OAc)2*2H₂O / chlorobenzene / 168 h / Heating

2: PBr₃ / tetrahydrofuran / 1 h / -20 °C

With cadmium(II) acetate; phosphorus tribromide; In tetrahydrofuran; chlorobenzene;
DOI:10.1055/s-2007-965938

Reference yield:

: 1585-17-7
2,4-bis(chloromethyl)mesitylene

: 943757-07-1
2-[3-(bromomethyl)-2,4,6-trimethylbenzyl]-4,4-dimethyl-4,5-dihydrooxazole

Guidance literature:: Multi-step reaction with 4 steps

1: 34 percent / dimethylsulfoxide

2: 99 percent / CaCO₃; H₂O / dioxane / 12 h / Heating

3: 52 percent / Cd(OAc)2*2H₂O / chlorobenzene / 168 h / Heating

4: PBr₃ / tetrahydrofuran / 1 h / -20 °C

With water; cadmium(II) acetate; phosphorus tribromide; calcium carbonate; In tetrahydrofuran; 1,4-dioxane; dimethyl sulfoxide; chlorobenzene;
DOI:10.1055/s-2007-965938