1-{3-[(4,4-dimethyl-4,5-dihydrooxazol-2-yl)methyl]-2,4,6-trimethylbenzyl}-3-methylimidazolium bromide

Base Information

Chemical Name:1-{3-[(4,4-dimethyl-4,5-dihydrooxazol-2-yl)methyl]-2,4,6-trimethylbenzyl}-3-methylimidazolium bromide
CAS No.:943756-97-6
Molecular Formula:Br*C₂₀H₂₈N₃O
Molecular Weight:406.366
Hs Code.:

Synonyms:1-{3-[(4,4-dimethyl-4,5-dihydrooxazol-2-yl)methyl]-2,4,6-trimethylbenzyl}-3-methylimidazolium bromide

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Chemical Property of 1-{3-[(4,4-dimethyl-4,5-dihydrooxazol-2-yl)methyl]-2,4,6-trimethylbenzyl}-3-methylimidazolium bromide

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Technology Process of 1-{3-[(4,4-dimethyl-4,5-dihydrooxazol-2-yl)methyl]-2,4,6-trimethylbenzyl}-3-methylimidazolium bromide

There total 5 articles about 1-{3-[(4,4-dimethyl-4,5-dihydrooxazol-2-yl)methyl]-2,4,6-trimethylbenzyl}-3-methylimidazolium bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 616-47-7
1-methyl-1H-imidazole

: 943757-07-1
2-[3-(bromomethyl)-2,4,6-trimethylbenzyl]-4,4-dimethyl-4,5-dihydrooxazole

: 943756-97-6
1-{3-[(4,4-dimethyl-4,5-dihydrooxazol-2-yl)methyl]-2,4,6-trimethylbenzyl}-3-methylimidazolium bromide

Guidance literature:: In N,N-dimethyl-formamide; at 80 ℃; for 12h;
DOI:10.1055/s-2007-965938

Reference yield:

: 943757-04-8
[3-(hydroxymethyl)-2,4,6-trimethylphenyl]acetonitrile

: 943756-97-6
1-{3-[(4,4-dimethyl-4,5-dihydrooxazol-2-yl)methyl]-2,4,6-trimethylbenzyl}-3-methylimidazolium bromide

Guidance literature:: Multi-step reaction with 3 steps

1: 52 percent / Cd(OAc)2*2H₂O / chlorobenzene / 168 h / Heating

2: PBr₃ / tetrahydrofuran / 1 h / -20 °C

3: 93 percent / dimethylformamide / 12 h / 80 °C

With cadmium(II) acetate; phosphorus tribromide; In tetrahydrofuran; N,N-dimethyl-formamide; chlorobenzene;
DOI:10.1055/s-2007-965938

Reference yield:

: 943757-06-0
{3-[(4,4-dimethyl-4,5-dihydrooxazol-2-yl)methyl]-2,4,6-trimethylphenyl}methanol

: 943756-97-6
1-{3-[(4,4-dimethyl-4,5-dihydrooxazol-2-yl)methyl]-2,4,6-trimethylbenzyl}-3-methylimidazolium bromide

Guidance literature:: Multi-step reaction with 2 steps

1: PBr₃ / tetrahydrofuran / 1 h / -20 °C

2: 93 percent / dimethylformamide / 12 h / 80 °C

With phosphorus tribromide; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1055/s-2007-965938