methyl (3R,4R)-3,4-dimethoxy-1-{[(3R,4R)-3,4-dimethoxy-1-(benzyloxycarbonylamino)-cyclopentyl]carbonylamino}cyclopentanecarboxylate

Base Information

Chemical Name:methyl (3R,4R)-3,4-dimethoxy-1-{[(3R,4R)-3,4-dimethoxy-1-(benzyloxycarbonylamino)-cyclopentyl]carbonylamino}cyclopentanecarboxylate
CAS No.:1380078-02-3
Molecular Formula:C₂₅H₃₆N₂O₉
Molecular Weight:508.569
Hs Code.:

Synonyms:methyl (3R,4R)-3,4-dimethoxy-1-{[(3R,4R)-3,4-dimethoxy-1-(benzyloxycarbonylamino)-cyclopentyl]carbonylamino}cyclopentanecarboxylate

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Chemical Property of methyl (3R,4R)-3,4-dimethoxy-1-{[(3R,4R)-3,4-dimethoxy-1-(benzyloxycarbonylamino)-cyclopentyl]carbonylamino}cyclopentanecarboxylate

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Technology Process of methyl (3R,4R)-3,4-dimethoxy-1-{[(3R,4R)-3,4-dimethoxy-1-(benzyloxycarbonylamino)-cyclopentyl]carbonylamino}cyclopentanecarboxylate

There total 7 articles about methyl (3R,4R)-3,4-dimethoxy-1-{[(3R,4R)-3,4-dimethoxy-1-(benzyloxycarbonylamino)-cyclopentyl]carbonylamino}cyclopentanecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1236286-57-9,289886-42-6
H-(R,R)-Ac₅cdOM-OMe

: 1380078-01-2
(3R,4R)-1-benzyloxycarbonylamino-3,4-(dimethoxy)cyclopentanecarboxylic acid

: 1380078-02-3
methyl (3R,4R)-3,4-dimethoxy-1-{[(3R,4R)-3,4-dimethoxy-1-(benzyloxycarbonylamino)-cyclopentyl]carbonylamino}cyclopentanecarboxylate

Guidance literature:: With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In acetonitrile; at 20 ℃; for 60h;
DOI:10.1002/chem.201102902

Reference yield:

: C₁₀H₁₅NO₅

: 1380078-02-3
methyl (3R,4R)-3,4-dimethoxy-1-{[(3R,4R)-3,4-dimethoxy-1-(benzyloxycarbonylamino)-cyclopentyl]carbonylamino}cyclopentanecarboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: benzene / 6 h / Reflux

2: 5%-palladium/activated carbon; hydrogen / methanol / 12 h

3: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / acetonitrile / 60 h / 20 °C

With 5%-palladium/activated carbon; hydrogen; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In methanol; acetonitrile; benzene;
DOI:10.1002/chem.201102902

Reference yield:

: 1380078-00-1
methyl (3R,4R)-1-benzyloxycarbonylamino-3,4-(dimethoxy)cyclopentanecarboxylate

: 1380078-02-3
methyl (3R,4R)-3,4-dimethoxy-1-{[(3R,4R)-3,4-dimethoxy-1-(benzyloxycarbonylamino)-cyclopentyl]carbonylamino}cyclopentanecarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: 5%-palladium/activated carbon; hydrogen / methanol / 12 h

2: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / acetonitrile / 60 h / 20 °C

With 5%-palladium/activated carbon; hydrogen; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In methanol; acetonitrile;
DOI:10.1002/chem.201102902