1-(2,4-Dichloro-phenyl)-2-imidazol-1-yl-ethanone O-(2-chloro-benzo[b]thiophen-3-ylmethyl)-oxime

Base Information

• Chemical Name: 1-(2,4-Dichloro-phenyl)-2-imidazol-1-yl-ethanone O-(2-chloro-benzo[b]thiophen-3-ylmethyl)-oxime
• CAS No.: 99592-27-5
• Molecular Formula: C₂₀H₁₄Cl₃N₃OS
• Molecular Weight: 450.776

Synonyms:1-(2,4-Dichloro-phenyl)-2-imidazol-1-yl-ethanone O-(2-chloro-benzo[b]thiophen-3-ylmethyl)-oxime

Chemical Property of 1-(2,4-Dichloro-phenyl)-2-imidazol-1-yl-ethanone O-(2-chloro-benzo[b]thiophen-3-ylmethyl)-oxime

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Technology Process of 1-(2,4-Dichloro-phenyl)-2-imidazol-1-yl-ethanone O-(2-chloro-benzo[b]thiophen-3-ylmethyl)-oxime

There total 2 articles about 1-(2,4-Dichloro-phenyl)-2-imidazol-1-yl-ethanone O-(2-chloro-benzo[b]thiophen-3-ylmethyl)-oxime which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

3-bromomethyl-2-chloro-benzothiophene (83450-19-5) + (Z)-1-(2,4-Dichlorophenyl)-2-(1H-imidazol-1-yl)ethanone oxime (100220-48-2) → 1-(2,4-Dichloro-phenyl)-2-imidazol-1-yl-ethanone O-(2-chloro-benzo[b]thiophen-3-ylmethyl)-oxime (99592-27-5)

Guidance literature:

With potassium hydroxide; In acetone; for 1.5h; Ambient temperature;

Reference yield: 86.0%

3-bromomethyl-2-chloro-benzothiophene (83450-19-5) + (Z)-1-(2,4-dichlorophenyl)-2-(1H-imidazol-1-yl)-ethanone oxime (64211-06-9) → 1-(2,4-Dichloro-phenyl)-2-imidazol-1-yl-ethanone O-(2-chloro-benzo[b]thiophen-3-ylmethyl)-oxime (99592-27-5)

Guidance literature:

With potassium hydroxide; In acetone; for 1.5h; -55 deg C to RT;;

Reference yield: 63.0%

1-(2,4-Dichloro-phenyl)-2-imidazol-1-yl-ethanone O-(2-chloro-benzo[b]thiophen-3-ylmethyl)-oxime (99592-27-5) → 1-(2,4-Dichloro-phenyl)-2-imidazol-1-yl-ethanone O-(2-chloro-benzo[b]thiophen-3-ylmethyl)-oxime; compound with nitric acid (99592-29-7)

Guidance literature:

With nitric acid; In acetone;

upstream raw materials:

3-bromomethyl-2-chloro-benzothiophene

(Z)-1-(2,4-dichlorophenyl)-2-(1H-imidazol-1-yl)-ethanone oxime

(Z)-1-(2,4-Dichlorophenyl)-2-(1H-imidazol-1-yl)ethanone oxime

Downstream raw materials:

1-(2,4-Dichloro-phenyl)-2-imidazol-1-yl-ethanone O-(2-chloro-benzo[b]thiophen-3-ylmethyl)-oxime; compound with nitric acid

1-(2,4-Dichloro-phenyl)-2-imidazol-1-yl-ethanone O-(2-chloro-benzo[b]thiophen-3-ylmethyl)-oxime; compound with naphthalene-1,5-disulfonic acid

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