1-(2,4-Dichloro-phenyl)-2-imidazol-1-yl-ethanone O-(2-chloro-benzo[b]thiophen-3-ylmethyl)-oxime; compound with naphthalene-1,5-disulfonic acid

Base Information

• Chemical Name: 1-(2,4-Dichloro-phenyl)-2-imidazol-1-yl-ethanone O-(2-chloro-benzo[b]thiophen-3-ylmethyl)-oxime; compound with naphthalene-1,5-disulfonic acid
• CAS No.: 99592-28-6
• Molecular Formula: C₁₀H₈O₆S₂*2C₂₀H₁₄Cl₃N₃OS
• Molecular Weight: 1189.85

Synonyms:

Chemical Property of 1-(2,4-Dichloro-phenyl)-2-imidazol-1-yl-ethanone O-(2-chloro-benzo[b]thiophen-3-ylmethyl)-oxime; compound with naphthalene-1,5-disulfonic acid

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Technology Process of 1-(2,4-Dichloro-phenyl)-2-imidazol-1-yl-ethanone O-(2-chloro-benzo[b]thiophen-3-ylmethyl)-oxime; compound with naphthalene-1,5-disulfonic acid

There total 3 articles about 1-(2,4-Dichloro-phenyl)-2-imidazol-1-yl-ethanone O-(2-chloro-benzo[b]thiophen-3-ylmethyl)-oxime; compound with naphthalene-1,5-disulfonic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

1-(2,4-Dichloro-phenyl)-2-imidazol-1-yl-ethanone O-(2-chloro-benzo[b]thiophen-3-ylmethyl)-oxime (99592-27-5) + naphthalene-1,5-disulfonate (81-04-9) → 1-(2,4-Dichloro-phenyl)-2-imidazol-1-yl-ethanone O-(2-chloro-benzo[b]thiophen-3-ylmethyl)-oxime; compound with naphthalene-1,5-disulfonic acid (99592-28-6,104907-73-5,142371-74-2)

Guidance literature:

In ethanol; water; Ambient temperature;

Reference yield:

3-bromomethyl-2-chloro-benzothiophene (83450-19-5) → 1-(2,4-Dichloro-phenyl)-2-imidazol-1-yl-ethanone O-(2-chloro-benzo[b]thiophen-3-ylmethyl)-oxime; compound with naphthalene-1,5-disulfonic acid (99592-28-6,104907-73-5,142371-74-2)

Guidance literature:

Multi-step reaction with 2 steps

1: 86 percent / potassium hydroxide / acetone / 1.5 h / Ambient temperature

2: 52 percent / ethanol; H₂O / Ambient temperature

With potassium hydroxide; In ethanol; water; acetone;

Reference yield:

(Z)-1-(2,4-Dichlorophenyl)-2-(1H-imidazol-1-yl)ethanone oxime (100220-48-2) → 1-(2,4-Dichloro-phenyl)-2-imidazol-1-yl-ethanone O-(2-chloro-benzo[b]thiophen-3-ylmethyl)-oxime; compound with naphthalene-1,5-disulfonic acid (99592-28-6,104907-73-5,142371-74-2)

Guidance literature:

Multi-step reaction with 2 steps

1: 86 percent / potassium hydroxide / acetone / 1.5 h / Ambient temperature

2: 52 percent / ethanol; H₂O / Ambient temperature

With potassium hydroxide; In ethanol; water; acetone;

upstream raw materials:

1-(2,4-Dichloro-phenyl)-2-imidazol-1-yl-ethanone O-(2-chloro-benzo[b]thiophen-3-ylmethyl)-oxime

naphthalene-1,5-disulfonate

3-bromomethyl-2-chloro-benzothiophene

(Z)-1-(2,4-Dichlorophenyl)-2-(1H-imidazol-1-yl)ethanone oxime

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