2-(2,4,6-tribromo-3-methoxyphenyl)ethanamine

Base Information

Chemical Name:2-(2,4,6-tribromo-3-methoxyphenyl)ethanamine
CAS No.:1359715-06-2
Molecular Formula:C₉H₁₀Br₃NO
Molecular Weight:387.897
Hs Code.:

Synonyms:2-(2,4,6-tribromo-3-methoxyphenyl)ethanamine

Suppliers and Price of 2-(2,4,6-tribromo-3-methoxyphenyl)ethanamine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of 2-(2,4,6-tribromo-3-methoxyphenyl)ethanamine

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of 2-(2,4,6-tribromo-3-methoxyphenyl)ethanamine

There total 3 articles about 2-(2,4,6-tribromo-3-methoxyphenyl)ethanamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 2039-67-0
2-(3-methoxyphenyl)-1-ethanamine

: 1359715-06-2
2-(2,4,6-tribromo-3-methoxyphenyl)ethanamine

Guidance literature:: With hydrogenchloride; bromine; acetic acid; for 3h;
DOI:10.1016/j.ejmech.2013.12.050

Reference yield: 82.0%

: 487027-13-4
(E)-1,3,5-tribromo-2-methoxy-4-(2-nitrovinyl)benzene

: 1359715-06-2
2-(2,4,6-tribromo-3-methoxyphenyl)ethanamine

Guidance literature:: With sodium tetrahydroborate; boron trifluoride diethyl etherate; In tetrahydrofuran; for 7.5h; Reflux;
DOI:10.1021/jo3000173

Reference yield:

: 1359715-22-2
C₉H₈Br₃NO₄

: 1359715-06-2
2-(2,4,6-tribromo-3-methoxyphenyl)ethanamine

Guidance literature:: Multi-step reaction with 2 steps

1: sulfuric acid / 1,2-dichloro-ethane / 1.33 h / 85 - 90 °C

2: sodium tetrahydroborate; boron trifluoride diethyl etherate / tetrahydrofuran / 7.5 h / Reflux

With sodium tetrahydroborate; sulfuric acid; boron trifluoride diethyl etherate; In tetrahydrofuran; 1,2-dichloro-ethane;
DOI:10.1021/jo3000173