neodymium(III) fluoride oxalate

Base Information

• Chemical Name: neodymium(III) fluoride oxalate
• CAS No.: 732223-53-9
• Molecular Formula: C₂O₄*F*Nd
• Molecular Weight: 251.258
• Mol file: 732223-53-9.mol

Synonyms:neodymium(III) fluoride oxalate

Chemical Property of neodymium(III) fluoride oxalate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of neodymium(III) fluoride oxalate

There total 2 articles about neodymium(III) fluoride oxalate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

sodium oxalate (62-76-0) + sodium fluoride (7681-49-4) + neodymium(III) nitrate (16454-60-7) → neodymium(III) fluoride (13709-42-7) + neodymium(III) fluoride oxalate (732223-53-9)

Guidance literature:

In water; Ln(NO3)3 soln. is added slowly to a soln. containing stoich. quantitiesof NaF and Na2C2O4 (molar ratio 2:1:2.5), mixt. is stirred at 50-66°C and heated for about 6 h (pH 5); ppt. is filtered off, washed with water and then with acetone and driedin air, elem. anal.;

Reference yield:

hydrogen fluoride (7664-39-3,12381-92-9,32057-09-3,74835-82-8) + oxalic acid (144-62-7,97993-78-7) + neodymium(III) nitrate (16454-60-7) → neodymium(III) fluoride (13709-42-7) + neodymium(III) fluoride oxalate (732223-53-9)

Guidance literature:

In water; Ln(NO3)3 soln. is added slowly to a soln. containing stoich. quantitiesof HF and H2C2O4 (molar ratio 2:1:2.5), mixt. is stirred at 50-66°C and heated for about 6 h (pH 5); ppt. is filtered off, washed with water and then with acetone and driedin air, elem. anal.;

upstream raw materials:

sodium oxalate

sodium fluoride

neodymium(III) nitrate

hydrogen fluoride