3-[(3-bromopropyl)oxy]-4-methylthiobenzenemethanol

Base Information

Chemical Name:3-[(3-bromopropyl)oxy]-4-methylthiobenzenemethanol
CAS No.:875581-86-5
Molecular Formula:C₁₁H₁₅BrO₂S
Molecular Weight:291.209
Hs Code.:

Synonyms:3-[(3-bromopropyl)oxy]-4-methylthiobenzenemethanol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-[(3-bromopropyl)oxy]-4-methylthiobenzenemethanol

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Technology Process of 3-[(3-bromopropyl)oxy]-4-methylthiobenzenemethanol

There total 1 articles about 3-[(3-bromopropyl)oxy]-4-methylthiobenzenemethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 3-hydroxy-4-methylthiobenzyl alcohol

: 109-64-8
1,3-dibromo-propane

: 875581-86-5
3-[(3-bromopropyl)oxy]-4-methylthiobenzenemethanol

Guidance literature:: With potassium carbonate; In acetone; for 24h; Heating;
DOI:10.1039/b510675c

Reference yield: 90.0%

: 875581-86-5
3-[(3-bromopropyl)oxy]-4-methylthiobenzenemethanol

: 875581-87-6
3-[(3-iodopropyl)oxy]-4-methylthiobenzenemethanol

Guidance literature:: With sodium iodide; In acetone; at 40 ℃; for 2h;
DOI:10.1039/b510675c

Reference yield:

: 875581-86-5
3-[(3-bromopropyl)oxy]-4-methylthiobenzenemethanol

: M-(+)-2,7,13-tris[3-[5-(hydroxymethyl)-2-thiomethylphenoxy]propyloxy]-3,8,13-trithiomethyl-10,15-dihydro-5H-tribenzo[a,d,g]cyclononene

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / NaI / acetone / 2 h / 40 °C

2: 36 percent / NaOH / dimethylformamide; H₂O; hexamethylphosphoric acid triamide / 20 °C

With sodium hydroxide; sodium iodide; In N,N,N,N,N,N-hexamethylphosphoric triamide; water; N,N-dimethyl-formamide; acetone;
DOI:10.1039/b510675c