3-[2-acetamido-2,2-di-(ethoxycarbonyl)-ethyl]-6-methoxy-2-phenylimidazoimidazo[1,2-a]pyridine

Base Information

Chemical Name:3-[2-acetamido-2,2-di-(ethoxycarbonyl)-ethyl]-6-methoxy-2-phenylimidazoimidazo[1,2-a]pyridine
CAS No.:1335061-33-0
Molecular Formula:C₂₄H₂₇N₃O₆
Molecular Weight:453.495
Hs Code.:

Synonyms:3-[2-acetamido-2,2-di-(ethoxycarbonyl)-ethyl]-6-methoxy-2-phenylimidazoimidazo[1,2-a]pyridine

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Chemical Property of 3-[2-acetamido-2,2-di-(ethoxycarbonyl)-ethyl]-6-methoxy-2-phenylimidazoimidazo[1,2-a]pyridine

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Technology Process of 3-[2-acetamido-2,2-di-(ethoxycarbonyl)-ethyl]-6-methoxy-2-phenylimidazoimidazo[1,2-a]pyridine

There total 5 articles about 3-[2-acetamido-2,2-di-(ethoxycarbonyl)-ethyl]-6-methoxy-2-phenylimidazoimidazo[1,2-a]pyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: 1335061-32-9
1-(6-methoxy-2-phenylimidazo[1,2-a]pyridin-3-yl)-N,N,N-trimethyl methanaminium iodide

: 1068-90-2
2-acetylaminomalonic acid diethyl ester

: 1335061-33-0
3-[2-acetamido-2,2-di-(ethoxycarbonyl)-ethyl]-6-methoxy-2-phenylimidazoimidazo[1,2-a]pyridine

Guidance literature:: With potassium carbonate; In acetone; for 48h; Reflux;
DOI:10.1016/j.ejmech.2011.06.030

Reference yield:

: 1335061-31-8
3-(N,N-dimethylaminomethyl)-6-methoxy-2-phenylimidazo[1,2-a]pyridine

: 1335061-33-0
3-[2-acetamido-2,2-di-(ethoxycarbonyl)-ethyl]-6-methoxy-2-phenylimidazoimidazo[1,2-a]pyridine

Guidance literature:: Multi-step reaction with 2 steps

1: methanol / 8 h / 20 °C

2: potassium carbonate / acetone / 48 h / Reflux

With potassium carbonate; In methanol; acetone;
DOI:10.1016/j.ejmech.2011.06.030

Reference yield:

: 1072-97-5
5-bromo-2-pyridylamine

: 1335061-33-0
3-[2-acetamido-2,2-di-(ethoxycarbonyl)-ethyl]-6-methoxy-2-phenylimidazoimidazo[1,2-a]pyridine

Guidance literature:: Multi-step reaction with 5 steps

1: sodium hydrogencarbonate / ethanol / Reflux

2: 1,10-Phenanthroline; caesium carbonate; copper(I) bromide / 24 h / 110 °C

3: acetonitrile / 20 - 70 °C

4: methanol / 8 h / 20 °C

5: potassium carbonate / acetone / 48 h / Reflux

With 1,10-Phenanthroline; sodium hydrogencarbonate; potassium carbonate; caesium carbonate; copper(I) bromide; In methanol; ethanol; acetone; acetonitrile;
DOI:10.1016/j.ejmech.2011.06.030