N-(4-chlorophenyl)-N-methylcinnamamide

Base Information

Chemical Name:N-(4-chlorophenyl)-N-methylcinnamamide
CAS No.:1507357-41-6
Molecular Formula:C₁₆H₁₄ClNO
Molecular Weight:271.746
Hs Code.:

Synonyms:N-(4-chlorophenyl)-N-methylcinnamamide

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Chemical Property of N-(4-chlorophenyl)-N-methylcinnamamide

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Technology Process of N-(4-chlorophenyl)-N-methylcinnamamide

There total 4 articles about N-(4-chlorophenyl)-N-methylcinnamamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 591-50-4
iodobenzene

: 3-chloro-N-(4-chlorophenyl)-N-methylpropanamide

: 1507357-41-6
N-(4-chlorophenyl)-N-methylcinnamamide

Guidance literature:: With palladium diacetate; potassium carbonate; triphenylphosphine; In N,N-dimethyl-formamide; at 20 - 90 ℃; for 16h; under 750.075 Torr; Inert atmosphere;
DOI:10.1016/S1872-2067(14)60247-3

Reference yield: 57.0%

: 124-38-9,18923-20-1
carbon dioxide

: N-(4-chlorophenyl)-N-methylacrylamide

: 74-88-4
methyl iodide

: 98-80-6
phenylboronic acid

: 1507357-41-6
N-(4-chlorophenyl)-N-methylcinnamamide

: C₁₆H₁₆ClNO

: methyl 2-benzyl-3-((4-chlorophenyl)(methyl)amino)-3-oxopropanoate

Guidance literature:: carbon dioxide; N-(4-chlorophenyl)-N-methylacrylamide; phenylboronic acid; With chloro(1,5-cyclooctadiene)rhodium(I) dimer; N,N,N',N'',N'''-pentamethyldiethylenetriamine; silver trifluoromethanesulfonate; caesium carbonate; In N,N-dimethyl acetamide; at 60 ℃; for 24h; Sealed tube; Green chemistry;

methyl iodide; With potassium carbonate; In N,N-dimethyl acetamide; at 60 ℃; for 2h; regioselective reaction; Green chemistry;
DOI:10.1039/d0gc02667k

Reference yield:

: 621-82-9
Cinnamic acid

: 1507357-41-6
N-(4-chlorophenyl)-N-methylcinnamamide

Guidance literature:: Multi-step reaction with 2 steps

1: thionyl chloride / 3 h / 60 °C

2: dichloromethane / 1 h / 20 °C

With thionyl chloride; In dichloromethane;
DOI:10.1021/ol403196h