4-(4-benzhydryl-2-oxo-oxazolidine-3-carbonyl)-pent-4-enoic acid tert-butyl ester

Base Information

Chemical Name:4-(4-benzhydryl-2-oxo-oxazolidine-3-carbonyl)-pent-4-enoic acid tert-butyl ester
CAS No.:864682-95-1
Molecular Formula:C₂₆H₂₉NO₅
Molecular Weight:435.52
Hs Code.:

Synonyms:4-(4-benzhydryl-2-oxo-oxazolidine-3-carbonyl)-pent-4-enoic acid tert-butyl ester

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Chemical Property of 4-(4-benzhydryl-2-oxo-oxazolidine-3-carbonyl)-pent-4-enoic acid tert-butyl ester

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Technology Process of 4-(4-benzhydryl-2-oxo-oxazolidine-3-carbonyl)-pent-4-enoic acid tert-butyl ester

There total 6 articles about 4-(4-benzhydryl-2-oxo-oxazolidine-3-carbonyl)-pent-4-enoic acid tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 864682-99-5
2-methylene-pentanedioic acid 1-benzotriazol-1-yl ester 5-tert-butyl ester

: C₁₆H₁₄NO₂^(1-)*Li⁽¹⁺⁾

: 864682-95-1
4-(4-benzhydryl-2-oxo-oxazolidine-3-carbonyl)-pent-4-enoic acid tert-butyl ester

Guidance literature:: In tetrahydrofuran; hexane; at -78 - 20 ℃;
DOI:10.1021/jo0507439

Reference yield:

: 1663-39-4,25232-27-3
tert-Butyl acrylate

: 864682-95-1
4-(4-benzhydryl-2-oxo-oxazolidine-3-carbonyl)-pent-4-enoic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 6 steps

1: 83 percent / NaH / tetrahydrofuran / 20 °C

2: 100 percent / hydrogen / Pd/C / tetrahydrofuran / 5 h

3: H₂O / 2 h / Heating

4: 65 mg / HCl / ethyl acetate

5: 89 percent / DCC / tetrahydrofuran / 4 h / 20 °C

6: 84 percent / tetrahydrofuran; hexane / -78 - 20 °C

With hydrogenchloride; hydrogen; sodium hydride; dicyclohexyl-carbodiimide; palladium on activated charcoal; In tetrahydrofuran; hexane; water; ethyl acetate;
DOI:10.1021/jo0507439

Reference yield:

: 864683-12-5
2-benzyloxycarbonyl-pentanedioic acid 1-benzyl ester 5-tert-butyl ester

: 864682-95-1
4-(4-benzhydryl-2-oxo-oxazolidine-3-carbonyl)-pent-4-enoic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: 100 percent / hydrogen / Pd/C / tetrahydrofuran / 5 h

2: H₂O / 2 h / Heating

3: 65 mg / HCl / ethyl acetate

4: 89 percent / DCC / tetrahydrofuran / 4 h / 20 °C

5: 84 percent / tetrahydrofuran; hexane / -78 - 20 °C

With hydrogenchloride; hydrogen; dicyclohexyl-carbodiimide; palladium on activated charcoal; In tetrahydrofuran; hexane; water; ethyl acetate;
DOI:10.1021/jo0507439