benzoic acid 3-{3-{3-[3-benzyloxymethyl-5-(3-methyl-benzyloxy)-phenoxy]-propoxy}-5-[4-bromo-3-(3-bromo-benzyloxy)-5-decyloxy-benzyloxy]-benzyloxy}-5-bromo-phenyl ester

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Chemical Name:benzoic acid 3-{3-{3-[3-benzyloxymethyl-5-(3-methyl-benzyloxy)-phenoxy]-propoxy}-5-[4-bromo-3-(3-bromo-benzyloxy)-5-decyloxy-benzyloxy]-benzyloxy}-5-bromo-phenyl ester
CAS No.:692205-23-5
Molecular Formula:C₆₉H₇₁Br₃O₁₀
Molecular Weight:1300.03
Hs Code.:

benzoic acid 3-{3-{3-[3-benzyloxymethyl-5-(3-methyl-benzyloxy)-phenoxy]-propoxy}-5-[4-bromo-3-(3-bromo-benzyloxy)-5-decyloxy-benzyloxy]-benzyloxy}-5-bromo-phenyl ester

Synonyms:benzoic acid 3-{3-{3-[3-benzyloxymethyl-5-(3-methyl-benzyloxy)-phenoxy]-propoxy}-5-[4-bromo-3-(3-bromo-benzyloxy)-5-decyloxy-benzyloxy]-benzyloxy}-5-bromo-phenyl ester

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Chemical Property of benzoic acid 3-{3-{3-[3-benzyloxymethyl-5-(3-methyl-benzyloxy)-phenoxy]-propoxy}-5-[4-bromo-3-(3-bromo-benzyloxy)-5-decyloxy-benzyloxy]-benzyloxy}-5-bromo-phenyl ester

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Technology Process of benzoic acid 3-{3-{3-[3-benzyloxymethyl-5-(3-methyl-benzyloxy)-phenoxy]-propoxy}-5-[4-bromo-3-(3-bromo-benzyloxy)-5-decyloxy-benzyloxy]-benzyloxy}-5-bromo-phenyl ester

There total 22 articles about benzoic acid 3-{3-{3-[3-benzyloxymethyl-5-(3-methyl-benzyloxy)-phenoxy]-propoxy}-5-[4-bromo-3-(3-bromo-benzyloxy)-5-decyloxy-benzyloxy]-benzyloxy}-5-bromo-phenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 692205-18-8
3-hydroxy-5-(benzoyloxy)bromobenzene

: 692205-13-3
5-(3-{3-[3-Benzyloxymethyl-5-(3-methyl-benzyloxy)-phenoxy]-propoxy}-5-bromomethyl-phenoxymethyl)-2-bromo-1-(3-bromo-benzyloxy)-3-decyloxy-benzene

: 692205-23-5
benzoic acid 3-{3-{3-[3-benzyloxymethyl-5-(3-methyl-benzyloxy)-phenoxy]-propoxy}-5-[4-bromo-3-(3-bromo-benzyloxy)-5-decyloxy-benzyloxy]-benzyloxy}-5-bromo-phenyl ester

Guidance literature:: With 18-crown-6 ether; potassium carbonate; In tetrahydrofuran; for 12h; Heating;
DOI:10.1021/jo049878p

Reference yield:

: 2050-77-3
Iododecane

: 692205-23-5
benzoic acid 3-{3-{3-[3-benzyloxymethyl-5-(3-methyl-benzyloxy)-phenoxy]-propoxy}-5-[4-bromo-3-(3-bromo-benzyloxy)-5-decyloxy-benzyloxy]-benzyloxy}-5-bromo-phenyl ester

Guidance literature:: Multi-step reaction with 8 steps

1: potassium carbonate; 18-crown-6 / acetone / 12 h / Heating

2: borane-dimethyl sulfide complex / tetrahydrofuran / 8 h / Heating

3: 87 percent / triphenylphosphine; N-bromosuccinimide / tetrahydrofuran / 20 °C

4: potassium carbonate; 18-crown-6 / tetrahydrofuran / 12 h / Heating

5: borane-dimethyl sulfide complex / tetrahydrofuran / 8 h / Heating

6: 90 percent / potassium carbonate; 18-crown-6 / acetone / 12 h / Heating

7: 96 percent / triphenylphosphine; N-bromosuccinimide / tetrahydrofuran / 20 °C

8: 55 percent / potassium carbonate; 18-crown-6 / tetrahydrofuran / 12 h / Heating

With N-Bromosuccinimide; 18-crown-6 ether; dimethylsulfide borane complex; potassium carbonate; triphenylphosphine; In tetrahydrofuran; acetone;
DOI:10.1021/jo049878p

Reference yield:

: 620-13-3
1-bromomethyl-3-methyl-benzene

: 692205-23-5
benzoic acid 3-{3-{3-[3-benzyloxymethyl-5-(3-methyl-benzyloxy)-phenoxy]-propoxy}-5-[4-bromo-3-(3-bromo-benzyloxy)-5-decyloxy-benzyloxy]-benzyloxy}-5-bromo-phenyl ester

Guidance literature:: Multi-step reaction with 7 steps

1.1: 79 percent / potassium carbonate; 18-crown-6 / acetone / 12 h / Heating

2.1: 93 percent / sodium hydride; 18-crown-6 / tetrahydrofuran / 20 °C

3.1: 9-BBN / tetrahydrofuran / 4 h / 20 °C

3.2: 92 percent / sodium hydroxide; hydrogen peroxide / H₂O; tetrahydrofuran / 2 h / 50 °C

4.1: 72 percent / triphenylphosphine; N-bromosuccinimide / tetrahydrofuran / 20 °C

5.1: 90 percent / potassium carbonate; 18-crown-6 / acetone / 12 h / Heating

6.1: 96 percent / triphenylphosphine; N-bromosuccinimide / tetrahydrofuran / 20 °C

7.1: 55 percent / potassium carbonate; 18-crown-6 / tetrahydrofuran / 12 h / Heating

With N-Bromosuccinimide; 9-borabicyclo[3.3.1]nonane dimer; 18-crown-6 ether; sodium hydride; potassium carbonate; triphenylphosphine; In tetrahydrofuran; acetone;
DOI:10.1021/jo049878p