3-[(phosphonic acid diethyl ester)-methyl]-5-(2-methyl-benzyloxy)-benzoic acid methyl ester

Base Information

Chemical Name:3-[(phosphonic acid diethyl ester)-methyl]-5-(2-methyl-benzyloxy)-benzoic acid methyl ester
CAS No.:1282521-32-7
Molecular Formula:C₂₁H₂₇O₆P
Molecular Weight:406.416
Hs Code.:

Synonyms:3-[(phosphonic acid diethyl ester)-methyl]-5-(2-methyl-benzyloxy)-benzoic acid methyl ester

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Chemical Property of 3-[(phosphonic acid diethyl ester)-methyl]-5-(2-methyl-benzyloxy)-benzoic acid methyl ester

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Technology Process of 3-[(phosphonic acid diethyl ester)-methyl]-5-(2-methyl-benzyloxy)-benzoic acid methyl ester

There total 6 articles about 3-[(phosphonic acid diethyl ester)-methyl]-5-(2-methyl-benzyloxy)-benzoic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.2%

: 1282521-31-6
3-bromomethyl-5-(2-methyl-benzyloxy)-benzoic acid methyl ester

: 122-52-1
triethyl phosphite

: 1282521-32-7
3-[(phosphonic acid diethyl ester)-methyl]-5-(2-methyl-benzyloxy)-benzoic acid methyl ester

Guidance literature:: at 160 ℃; for 3h;

Reference yield:

: 89-92-9
2-methylbenzyl bromide

: 1282521-32-7
3-[(phosphonic acid diethyl ester)-methyl]-5-(2-methyl-benzyloxy)-benzoic acid methyl ester

Guidance literature:: Multi-step reaction with 5 steps

1.1: potassium carbonate / N,N-dimethyl-formamide / 12 h / 150 °C

2.1: potassium hydroxide; methanol / 12 h / 100 °C

3.1: borane-THF / tetrahydrofuran / 12 h / 0 - 20 °C

3.2: 3 h / 0 °C

4.1: tribromide phosphate / tetrahydrofuran / 12 h / 0 - 20 °C

5.1: 3 h / 160 °C

With methanol; borane-THF; tribromide phosphate; potassium carbonate; potassium hydroxide; In tetrahydrofuran; N,N-dimethyl-formamide;

Reference yield:

: 13036-02-7
Dimethyl 5-hydroxyisophthalate

: 1282521-32-7
3-[(phosphonic acid diethyl ester)-methyl]-5-(2-methyl-benzyloxy)-benzoic acid methyl ester

Guidance literature:: Multi-step reaction with 5 steps

1.1: potassium carbonate / N,N-dimethyl-formamide / 12 h / 150 °C

2.1: potassium hydroxide; methanol / 12 h / 100 °C

3.1: borane-THF / tetrahydrofuran / 12 h / 0 - 20 °C

3.2: 3 h / 0 °C

4.1: tribromide phosphate / tetrahydrofuran / 12 h / 0 - 20 °C

5.1: 3 h / 160 °C

With methanol; borane-THF; tribromide phosphate; potassium carbonate; potassium hydroxide; In tetrahydrofuran; N,N-dimethyl-formamide;