N-((3-(chloromethyl)cyclohex-1-enyl)methyl)-4-methyl-N-(3-(4-nitrophenyl)prop-2-yn-1-yl)benzenesulfonamide

Base Information

Chemical Name:N-((3-(chloromethyl)cyclohex-1-enyl)methyl)-4-methyl-N-(3-(4-nitrophenyl)prop-2-yn-1-yl)benzenesulfonamide
CAS No.:1404440-24-9
Molecular Formula:C₂₄H₂₅ClN₂O₄S
Molecular Weight:472.993
Hs Code.:

Synonyms:N-((3-(chloromethyl)cyclohex-1-enyl)methyl)-4-methyl-N-(3-(4-nitrophenyl)prop-2-yn-1-yl)benzenesulfonamide

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Chemical Property of N-((3-(chloromethyl)cyclohex-1-enyl)methyl)-4-methyl-N-(3-(4-nitrophenyl)prop-2-yn-1-yl)benzenesulfonamide

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Technology Process of N-((3-(chloromethyl)cyclohex-1-enyl)methyl)-4-methyl-N-(3-(4-nitrophenyl)prop-2-yn-1-yl)benzenesulfonamide

There total 5 articles about N-((3-(chloromethyl)cyclohex-1-enyl)methyl)-4-methyl-N-(3-(4-nitrophenyl)prop-2-yn-1-yl)benzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: (±)-N-(((1S,5R,6S)-5-hydroxybicyclo[4.1.0]heptan-1-yl)methyl)-4-methyl-N-(3-(4-nitrophenyl)prop-2-yn-1-yl)benzenesulfonamide

: 1404440-24-9
N-((3-(chloromethyl)cyclohex-1-enyl)methyl)-4-methyl-N-(3-(4-nitrophenyl)prop-2-yn-1-yl)benzenesulfonamide

Guidance literature:: With iron(III) chloride; In dichloromethane; at -15 ℃; for 0.05h;
DOI:10.1021/jo301764g

Reference yield:

: 1354575-43-1
C₂₃H₂₄N₂O₅S

: 1404440-24-9
N-((3-(chloromethyl)cyclohex-1-enyl)methyl)-4-methyl-N-(3-(4-nitrophenyl)prop-2-yn-1-yl)benzenesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1: diethylzinc / dichloromethane; diethyl ether / 10 h / 0 - 30 °C

2: iron(III) chloride / dichloromethane / 0.05 h / -15 °C

With iron(III) chloride; diethylzinc; In diethyl ether; dichloromethane;
DOI:10.1021/jo301764g

Reference yield:

: 58775-64-7
3-[(methylthio)methyl]cyclohex-2-en-1-one

: 1404440-24-9
N-((3-(chloromethyl)cyclohex-1-enyl)methyl)-4-methyl-N-(3-(4-nitrophenyl)prop-2-yn-1-yl)benzenesulfonamide

Guidance literature:: Multi-step reaction with 5 steps

1: methyl iodide / dichloromethane / 72 h / 45 °C

2: potassium carbonate / acetone / 10 h / 20 °C

3: cerium(III) chloride heptahydrate; sodium tetrahydroborate / methanol / 1 h / 0 °C

4: diethylzinc / dichloromethane; diethyl ether / 10 h / 0 - 30 °C

5: iron(III) chloride / dichloromethane / 0.05 h / -15 °C

With iron(III) chloride; sodium tetrahydroborate; cerium(III) chloride heptahydrate; diethylzinc; potassium carbonate; methyl iodide; In methanol; diethyl ether; dichloromethane; acetone;
DOI:10.1021/jo301764g