(2S,3S)-methyl 3-[N-benzyl-hydroxyamino]-2-(tert-butyldimethylsiloxy)-3-[(S)-2,2-dimethyl-1,3-dioxolan-4-yl]propanoate

Base Information

Chemical Name:(2S,3S)-methyl 3-[N-benzyl-hydroxyamino]-2-(tert-butyldimethylsiloxy)-3-[(S)-2,2-dimethyl-1,3-dioxolan-4-yl]propanoate
CAS No.:898232-14-9
Molecular Formula:C₂₂H₃₇NO₆Si
Molecular Weight:439.624
Hs Code.:

Synonyms:(2S,3S)-methyl 3-[N-benzyl-hydroxyamino]-2-(tert-butyldimethylsiloxy)-3-[(S)-2,2-dimethyl-1,3-dioxolan-4-yl]propanoate

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Chemical Property of (2S,3S)-methyl 3-[N-benzyl-hydroxyamino]-2-(tert-butyldimethylsiloxy)-3-[(S)-2,2-dimethyl-1,3-dioxolan-4-yl]propanoate

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Technology Process of (2S,3S)-methyl 3-[N-benzyl-hydroxyamino]-2-(tert-butyldimethylsiloxy)-3-[(S)-2,2-dimethyl-1,3-dioxolan-4-yl]propanoate

There total 7 articles about (2S,3S)-methyl 3-[N-benzyl-hydroxyamino]-2-(tert-butyldimethylsiloxy)-3-[(S)-2,2-dimethyl-1,3-dioxolan-4-yl]propanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 898232-07-0
(2S,3S)-methyl 3-[N-benzyl-N-(trimethylsiloxy)amino]-2-(tert-butyldimethylsiloxy)-3-[(S)-2,2-dimethyl-1,3-dioxolan-4-yl]propanoate

: 898232-14-9
(2S,3S)-methyl 3-[N-benzyl-hydroxyamino]-2-(tert-butyldimethylsiloxy)-3-[(S)-2,2-dimethyl-1,3-dioxolan-4-yl]propanoate

Guidance literature:: With citric acid; In methanol; at 20 ℃; for 0.25h;
DOI:10.1021/jo060465t

Reference yield:

: 91190-38-4,111058-38-9,1165677-00-8
N-benzyl-2,3-O-isopropylidene-D-glyceraldehyde nitrone

: 150811-50-0
(E)-((2-((tert-butyldimethylsilyl)oxy)-1-methoxyvinyl)oxy)trimethylsilane

: 898232-17-2
(2R,3R)-methyl 3-[N-benzyl-hydroxyamino]-2-(tert-butyldimethylsiloxy)-3-[(S)-2,2-dimethyl-1,3-dioxolan-4-yl]propanoate

: (2R,3S)-3-(Benzyl-hydroxy-amino)-2-(tert-butyl-dimethyl-silanyloxy)-3-((S)-2,2-dimethyl-[1,3]dioxolan-4-yl)-propionic acid methyl ester

: (2S,3R)-3-(Benzyl-hydroxy-amino)-2-(tert-butyl-dimethyl-silanyloxy)-3-((S)-2,2-dimethyl-[1,3]dioxolan-4-yl)-propionic acid methyl ester

: 898232-14-9
(2S,3S)-methyl 3-[N-benzyl-hydroxyamino]-2-(tert-butyldimethylsiloxy)-3-[(S)-2,2-dimethyl-1,3-dioxolan-4-yl]propanoate

Guidance literature:: N-benzyl-2,3-O-isopropylidene-D-glyceraldehyde nitrone; (E)-((2-((tert-butyldimethylsilyl)oxy)-1-methoxyvinyl)oxy)trimethylsilane; With aluminium trichloride; In dichloromethane; at -78 ℃; for 3h;

With citric acid; In methanol; at 20 ℃; for 0.25h;
DOI:10.1021/jo060465t